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DOTA Functionalized Cross-Linked Small-Molecule Micelles for Theranostics Combining Magnetic Resonance Imaging and Chemotherapy
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    DOTA Functionalized Cross-Linked Small-Molecule Micelles for Theranostics Combining Magnetic Resonance Imaging and Chemotherapy
    Click to copy article linkArticle link copied!

    • Jianyue Feng
      Jianyue Feng
      College of Chemistry, Sichuan University, 29 Wangjiang Road, Chengdu 610064, China
      More by Jianyue Feng
    • Qiang Luo
      Qiang Luo
      Huaxi MR Research Center (HMRRC), Department of Radiology, West China Hospital, Sichuan University, Chengdu 610041, China
      More by Qiang Luo
    • Yun Chen
      Yun Chen
      National Engineering Research Center for Biomaterials, Sichuan University, 29 Wangjiang Road, Chengdu 610064, China
      More by Yun Chen
    • Bing Li
      Bing Li
      National Engineering Research Center for Biomaterials, Sichuan University, 29 Wangjiang Road, Chengdu 610064, China
      More by Bing Li
    • Kui Luo
      Kui Luo
      Huaxi MR Research Center (HMRRC), Department of Radiology, West China Hospital, Sichuan University, Chengdu 610041, China
      More by Kui Luo
    • Jingbo Lan*
      Jingbo Lan
      College of Chemistry, Sichuan University, 29 Wangjiang Road, Chengdu 610064, China
      *E-mail: [email protected]
      More by Jingbo Lan
    • Yunlong Yu
      Yunlong Yu
      National Engineering Research Center for Biomaterials, Sichuan University, 29 Wangjiang Road, Chengdu 610064, China
      More by Yunlong Yu
    • Shiyong Zhang*
      Shiyong Zhang
      College of Chemistry  and  National Engineering Research Center for Biomaterials, Sichuan University, 29 Wangjiang Road, Chengdu 610064, China
      *E-mail: [email protected]
    Other Access OptionsSupporting Information (1)

    Bioconjugate Chemistry

    Cite this: Bioconjugate Chem. 2018, 29, 10, 3402–3410
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acs.bioconjchem.8b00565
    Published September 10, 2018
    Copyright © 2018 American Chemical Society

    Abstract

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    Abstract Image

    Herein, a new theranostic nanoplatform was built by introducing DOTA on the surface of the cross-linked small molecular micelles. This nanoplatform consisted of three parts: (1) Hydrophobic alkyl chain functioned with alkenes as cross-linkable part to ensure the robust stability in vivo; (2) Hydrophilic DOTA for not only gadolinium ions complexion as MR imaging contrast agents but also platinum ions complexion as drug carriers; (3) Cisplatin as antitumor drug and MR imaging amplifier simultaneously. The metal loading content of the resulting Pt/Gd@DOTA-CSMs was up to 12 and 14 wt % for Gd(III) and Pt(II), respectively. The longitudinal relaxation rate of Gd@DOTA-CSMs (8.46 mM–1 s–1) was 2.6 times than that of the clinical Gd-DTPA (3.23 mM–1 s–1). When cisplatin was involved, not only great antitumor efficiency was achieved, but higher longitudinal relaxation rate of Pt/Gd@DOTA-CSMs (11.17 mM–1 s–1) was carried out due to the extension of rotational correlation time. The experiments of Balb/c mice bearing 4T1 xenograft indicated that Pt/Gd@DOTA-CSMs had better antitumor activity, lower side effect than clinically used cisplatin, and greater MR imaging than Gd-DTPA. All the results proved that the nanoplatform of DOTA-CSMs held remarkable potential in the field of therapeutics.

    Copyright © 2018 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.bioconjchem.8b00565.

    • Additional 1H NMR spectra, 13C NMR spectra of synthesized compounds, fluorescence spectra, and cytotoxicity assay (PDF)

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    Cited By

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    This article is cited by 13 publications.

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    2. Ying Chen, Yongchao Yao, Xueying Zhou, Chunyan Liao, Xin Dai, Jie Liu, Yunlong Yu, Shiyong Zhang. Cascade-Reaction-Based Nanodrug for Combined Chemo/Starvation/Chemodynamic Therapy against Multidrug-Resistant Tumors. ACS Applied Materials & Interfaces 2019, 11 (49) , 46112-46123. https://doi.org/10.1021/acsami.9b15848
    3. Yongchao Yao, Ying Chen, Yong Liu, Yuhong Zhu, Yuanming Liu, Shiyong Zhang. Facile Transfer of Reverse Micelles from the Organic to the Aqueous Phase for Mimicking Enzyme Catalysis and Imaging-Guided Cancer Therapy. Langmuir 2019, 35 (17) , 5871-5877. https://doi.org/10.1021/acs.langmuir.9b00607
    4. Daniele Paderni, Maria Voccia, Eleonora Macedi, Mauro Formica, Luca Giorgi, Lucia Caporaso, Vieri Fusi. A combined solid state, solution and DFT study of a dimethyl-cyclen-Pd( ii ) complex. Dalton Transactions 2024, 53 (34) , 14300-14314. https://doi.org/10.1039/D4DT01791A
    5. Giulia Ferrari, Ines Lopez-Martinez, Thomas Wanek, Claudia Kuntner, Diego Montagner. Recent Advances on Pt-Based Compounds for Theranostic Applications. Molecules 2024, 29 (15) , 3453. https://doi.org/10.3390/molecules29153453
    6. Subrata Santra, Mijanur Rahaman Molla. Small Molecule Based Core and Shell Cross-Linked Nanoassemblies: from Self-Assembly and Programmed Disassembly to Biological Applications. Chemical Communications 2024, https://doi.org/10.1039/D4CC03515A
    7. Lijiao Yang, Shaomin Song, Meihui Yin, Min Yang, Daoping Yan, Xiaohui Wan, Jipeng Xiao, Yuchen Jiang, Yongchao Yao, Jianbin Luo. Antibiotic-based small molecular micelles combined with photodynamic therapy for bacterial infections. Asian Journal of Pharmaceutical Sciences 2023, 18 (3) , 100810. https://doi.org/10.1016/j.ajps.2023.100810
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    9. Meghanath B. Shete, Tulshidas S. Patil, Ashwini S. Deshpande, Gaurav Saraogi, Nupur Vasdev, Mrudul Deshpande, Kuldeep Rajpoot, Rakesh Kumar Tekade. Current trends in theranostic nanomedicines. Journal of Drug Delivery Science and Technology 2022, 71 , 103280. https://doi.org/10.1016/j.jddst.2022.103280
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    12. Qian Zhang, Yun Chen, Ruilin Lu, Yongchao Yao, Chuanqi Li, Yunlong Yu, Shiyong Zhang. Cross-linked small-molecule capsules with excitation wavelength-dependent photoluminescence and high loading capacity: design, synthesis and application in imaging-guided drug delivery. Journal of Materials Chemistry B 2020, 8 (13) , 2719-2725. https://doi.org/10.1039/C9TB02465D
    13. Fuqing Xiang, Bing Li, Pengxiang Zhao, Jiangbing Tan, Yunlong Yu, Shiyong Zhang. Copper(I)‐Chelated Cross‐Linked Cyclen Micelles as a Nanocatalyst for Azide‐Alkyne Cycloaddition in Both Water and Cells. Advanced Synthesis & Catalysis 2019, 361 (21) , 5057-5062. https://doi.org/10.1002/adsc.201900773

    Bioconjugate Chemistry

    Cite this: Bioconjugate Chem. 2018, 29, 10, 3402–3410
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acs.bioconjchem.8b00565
    Published September 10, 2018
    Copyright © 2018 American Chemical Society

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