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    Environmentally Friendly in Situ Regeneration of Graphene Aerogel as a Model Conductive Adsorbent
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    † Key Laboratory of Pollution Processes and Environmental Criteria (Ministry of Education), Tianjin Key Laboratory of Environmental Remediation and Pollution Control, College of Environmental Science and Engineering, Nankai University, Tianjin 300071, China
    ‡ § ‡State Key Laboratory of Pollution Control and Resource Reuse, School of Environment and §Research Center for Environmental Nanotechnology (ReCENT), Nanjing University, Nanjing 210023, China
    *Guandao Gao Phone/fax: +86-25-89681675. E-mail: [email protected]
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    Environmental Science & Technology

    Cite this: Environ. Sci. Technol. 2018, 52, 2, 739–746
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    https://doi.org/10.1021/acs.est.7b02795
    Published December 15, 2017
    Copyright © 2017 American Chemical Society
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    Abstract

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    Adsorption is a classical process widely used in industry and environmental protection, and the regeneration of exhausted adsorbents, as the reverse process of adsorption, is vital to achieving a sustainable adsorption process. Chemical and thermal regeneration, which feature high costs and environmental side effects, are classical but not environmentally friendly methods. Herein, a new regeneration method based on an electrochemical process using graphene aerogel (GA) as a model conductive adsorbent was proposed. First, 3D GA was prepared to adsorb organic and inorganic pollutants, avoiding the inconvenience of using powdered graphene. Then, the exhausted GA was cleaned by the electrochemical desorption and degradation of adsorbed organic pollutants if undesired and the electrorepulsion of adsorbed metal ions in the absence of any additional chemicals, showing a high processing capability of 1.21 L g–1 GA h–1 and low energy consumption (∼0.2 kWh m–3 solution). The mechanisms involved in the electrochemistry-induced desorption process cover a decline in the GA adsorption performance depended on the electrochemically adjustable surface charge conditions, and the further repulsion and migration of adsorbates is subject to the strong in situ electric field. This work has important implications for the development of environmentally friendly regeneration processes and qualified adsorbents as well as the application of a green and efficient regeneration concept for traditional adsorption processes.

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acs.est.7b02795.

    • A schematic representation of the procedure for the preparation of GA samples. Figures showing XRD results, pore size distribution, BET, XPS O 1s spectra of samples, and the speciation of Cu2+ in aqueous solution under different pH simulated by visual MINTEQ. Tables showing the characterization of pores and functional groups, adsorption capacity of graphene, and O-to-C and functional group ratios. (PDF)

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    Cite this: Environ. Sci. Technol. 2018, 52, 2, 739–746
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acs.est.7b02795
    Published December 15, 2017
    Copyright © 2017 American Chemical Society
    Request reuse permissions

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