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Stretchable Carbon Nanotube Dilatometer for In Situ Swelling Detection of Lithium-Ion Batteries
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    Stretchable Carbon Nanotube Dilatometer for In Situ Swelling Detection of Lithium-Ion Batteries
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    • Leilei Wang
      Leilei Wang
      School of Mechanical Engineering, Yeungnam University, 280Daehak-ro, Gyeongsan, Gyeongbuk 38541, Republic of Korea
      More by Leilei Wang
    • Woohyuk Choi
      Woohyuk Choi
      School of Mechanical Engineering, Yeungnam University, 280Daehak-ro, Gyeongsan, Gyeongbuk 38541, Republic of Korea
      More by Woohyuk Choi
    • Kisoo Yoo
      Kisoo Yoo
      School of Mechanical Engineering, Yeungnam University, 280Daehak-ro, Gyeongsan, Gyeongbuk 38541, Republic of Korea
      More by Kisoo Yoo
    • Kanghyun Nam
      Kanghyun Nam
      School of Mechanical Engineering, Yeungnam University, 280Daehak-ro, Gyeongsan, Gyeongbuk 38541, Republic of Korea
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    • Tae Jo Ko*
      Tae Jo Ko
      School of Mechanical Engineering, Yeungnam University, 280Daehak-ro, Gyeongsan, Gyeongbuk 38541, Republic of Korea
      *Email: [email protected]
      More by Tae Jo Ko
    • Jungwook Choi*
      Jungwook Choi
      School of Mechanical Engineering, Yeungnam University, 280Daehak-ro, Gyeongsan, Gyeongbuk 38541, Republic of Korea
      *Email: [email protected]
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    ACS Applied Energy Materials

    Cite this: ACS Appl. Energy Mater. 2020, 3, 4, 3637–3644
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    https://doi.org/10.1021/acsaem.0c00114
    Published March 19, 2020
    Copyright © 2020 American Chemical Society

    Abstract

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    Advances in lithium-ion batteries (LIBs) have enabled the realization of lightweight power sources with high energy density, specific capacity, and cyclic stability. As LIBs are inherently subjected to thermomechanical stress during operation, their volume change can be indicative of their electrochemical reactions and safety status. In this study, a carbon nanotube (CNT)-based dilatometer that is stretchable and can be conformally mounted on the surface of LIBs has been developed for sensitive and in situ measurements of the LIB swelling. The CNTs form a percolation network on top of a thin elastomer and exhibit a positive gauge factor of ∼50 and a negative temperature coefficient of resistance of −0.075% K–1, enabling a quantitative extraction of the extent of swelling. As a result, both regular (∼50 μm swelling by lithiation/delithiation cycles) and irregular (a few millimeter swelling by abnormal gas evolution because of increased temperature) reactions of LIBs are successfully detected in real time. Unlike the conventional dilatometers that are complex, expensive, and bulky, the CNT sensor, because of its simplicity, portability, and sensitivity, is useful for understanding electrochemical reactions and preventing serious failures of portable LIBs, without disassembling them from the other components of the device.

    Copyright © 2020 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/acsaem.0c00114.

    • Mechanical property of PDMS; characterization of the LIB used for swelling measurements; characterization of the CNT sensor according to the CNT thickness; mechanical and thermal reliability of the CNT sensor; dependence of the coefficient of thermal expansion of PDMS on temperature; noise processing using RLS algorithm; and LIB swelling during regular charge and discharge cycles: irregular, irreversible, and thermomechanical swelling of the LIB (PDF)

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    Cited By

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    This article is cited by 13 publications.

    1. Yiting Sun, Hongfei Lu, Yang Jin. Experimental and Numerical Study on Mechanical Deformation Characteristics of Lithium Iron Phosphate Pouch Battery Modules under Overcharge Conditions. Energy & Fuels 2021, 35 (18) , 15172-15184. https://doi.org/10.1021/acs.energyfuels.1c02308
    2. Anyu Su, Shuoyuan Mao, Languang Lu, Xuebing Han, Minggao Ouyang. Implanted potential sensing separator enables smart battery internal state monitor and safety alert. eTransportation 2024, 22 , 100339. https://doi.org/10.1016/j.etran.2024.100339
    3. Seokwon Hong, Jihyun Bae, Byoung-Sun Lee. Designing PVdF-HFP/BTO Piezoelectric Sensor based Sensing System for Detecting Volume Expansion of Battery Cell. Ceramist 2024, 27 (1) , 61-74. https://doi.org/10.31613/ceramist.2024.27.1.03
    4. Fuqian Yang. Lithiation-induced swelling of electrodes. Journal of Energy Storage 2024, 75 , 109634. https://doi.org/10.1016/j.est.2023.109634
    5. Yao Lu, Xiaodan Wang, Shuoyuan Mao, Depeng Wang, Daoming Sun, Yukun Sun, Anyu Su, Chenzi Zhao, Xuebing Han, Kuijie Li, Xuning Feng, Xiang Liu, Xiangdong Kong, Languang Lu, Zhengyu Chu, Qiang Zhang, Minggao Ouyang. Smart batteries enabled by implanted flexible sensors. Energy & Environmental Science 2023, 16 (6) , 2448-2463. https://doi.org/10.1039/D3EE00695F
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    7. Soonjae Pyo, Youngkee Eun, Jaesam Sim, Kwanoh Kim, Jungwook Choi. Carbon nanotube-graphene hybrids for soft electronics, sensors, and actuators. Micro and Nano Systems Letters 2022, 10 (1) https://doi.org/10.1186/s40486-022-00151-w
    8. Leilei Wang, Jungwook Choi. Highly stretchable strain sensors with improved sensitivity enabled by a hybrid of carbon nanotube and graphene. Micro and Nano Systems Letters 2022, 10 (1) https://doi.org/10.1186/s40486-022-00160-9
    9. Heewon Choi, Nam-gyu Lim, Seong Jun Lee, Jungsoo Park. Numerical approach for lithium-ion battery performance considering various cathode active material composition for electric vehicles using 1D simulation. Journal of Mechanical Science and Technology 2021, 35 (6) , 2697-2705. https://doi.org/10.1007/s12206-021-0540-1
    10. Yumeng Wang, Xingsheng Li, Yue Hou, Chengri Yin, Zhenxing Yin. A review on structures, materials and applications of stretchable electrodes. Frontiers of Materials Science 2021, 15 (1) , 54-78. https://doi.org/10.1007/s11706-021-0537-9
    11. Shanpu Zheng, Shiping Jiang, Ying Luo, Baiqiang Xu, Wenfeng Hao. Guided wave imaging of thin lithium-ion pouch cell using scanning laser Doppler vibrometer. Ionics 2021, 27 (2) , 643-650. https://doi.org/10.1007/s11581-020-03869-y
    12. Mohamed Raghibi, Baokou Xiong, Satyajit Phadke, Mérièm Anouti. Role of the electrolyte in gas formation during the cycling of a Gr//NMC battery as a function of temperature: Solvent, salt, and ionic liquid effect.. Electrochimica Acta 2020, 362 , 137214. https://doi.org/10.1016/j.electacta.2020.137214
    13. Dongwoon Shin, Sun Choi, Jonghyun Kim, Abiral Regmi, Jiyoung Chang. Direct‐Printing of Functional Nanofibers on 3D Surfaces Using Self‐Aligning Nanojet in Near‐Field Electrospinning. Advanced Materials Technologies 2020, 5 (6) https://doi.org/10.1002/admt.202000232

    ACS Applied Energy Materials

    Cite this: ACS Appl. Energy Mater. 2020, 3, 4, 3637–3644
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acsaem.0c00114
    Published March 19, 2020
    Copyright © 2020 American Chemical Society

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