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    Research Article

    Rapid Large-Scale Assembly and Pattern Transfer of One-Dimensional Gold Nanorod Superstructures
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    † Center for Neutron Research, National Institute of Standards and Technology (NIST), Gaithersburg, Maryland 20899, United States
    ‡ Materials Science and Engineering Department, University of Maryland, College Park, Maryland 20742, United States
    § Biology and Soft Matter Division, Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831, United States
    ∥ Department of Macromolecular Science & Engineering, Case Western Reserve University, 10900 Euclid Avenue, Cleveland, Ohio 44106, United States
    ⊥ Department of Chemistry, University of Pennsylvania, 231 South 34th Street, Philadelphia, Pennsylvania 19104, United States
    # Center for Nanoscale Science and Technology, National Institute of Standards and Technology (NIST), Gaithersburg, Maryland 20899, United States
    ∇ Department of Electrical and Systems Engineering, University of Pennsylvania, 200 South 33rd Street, Philadelphia, Pennsylvania 19104, United States
    ○ Department of Materials Science & Engineering, University of Pennsylvania, 3231 Walnut Street, Philadelphia, Pennsylvania 19104, United States
    *E-mail: [email protected]
    *E-mail: [email protected]
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    ACS Applied Materials & Interfaces

    Cite this: ACS Appl. Mater. Interfaces 2017, 9, 30, 25513–25521
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    https://doi.org/10.1021/acsami.7b06273
    Published July 7, 2017
    Copyright © 2017 American Chemical Society
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    Abstract

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    The utility of gold nanorods for plasmonic applications largely depends on the relative orientation and proximity of the nanorods. Though side-by-side or chainlike nanorod morphologies have been previously demonstrated, a simple reliable method to obtain high-yield oriented gold nanorod assemblies remains a significant challenge. We present a facile, scalable approach which exploits meniscus drag, evaporative self-assembly, and van der Waals interactions to precisely position and orient gold nanorods over macroscopic areas of 1D nanostructured substrates. By adjusting the ratio of the nanorod diameter to the width of the nanochannels, we demonstrate the formation of two highly desired translationally ordered nanorod patterns. We further demonstrate a method to transfer the aligned nanorods into a polymer matrix which exhibits anisotropic optical properties, allowing for rapid fabrication and deployment of flexible optical and electronic materials in future nanoscale devices.

    Copyright © 2017 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/acsami.7b06273.

    • Nanostamp cross section, small-angle neutron scattering (SANS) characterization, SEM of PMMS imprint, discussion of dark field scattering spectroscopy results, and orientational analysis of SEM micrographs (PDF)

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    This article is cited by 27 publications.

    1. Jiapeng Zheng, Xizhe Cheng, Han Zhang, Xiaopeng Bai, Ruoqi Ai, Lei Shao, Jianfang Wang. Gold Nanorods: The Most Versatile Plasmonic Nanoparticles. Chemical Reviews 2021, 121 (21) , 13342-13453. https://doi.org/10.1021/acs.chemrev.1c00422
    2. Jaciara Bär, Anerise de Barros, Davi H. S. de Camargo, Mariane P. Pereira, Leandro Merces, Flavio Makoto Shimizu, Fernando A. Sigoli, Carlos César Bof Bufon, Italo Odone Mazali. Silicon Microchannel-Driven Raman Scattering Enhancement to Improve Gold Nanorod Functions as a SERS Substrate toward Single-Molecule Detection. ACS Applied Materials & Interfaces 2021, 13 (30) , 36482-36491. https://doi.org/10.1021/acsami.1c08480
    3. Makoto Tago, Mihiro Takasaki, Yuki Tokura, Yuya Oaki, Hiroaki Imai. Self-Assembly of 2D Nematic and Random Arrays of Sterically Stabilized Nanoscale Rods with and without Evaporation. Langmuir 2021, 37 (21) , 6533-6539. https://doi.org/10.1021/acs.langmuir.1c00789
    4. Maria Blanco-Formoso, Nicolas Pazos-Perez, Ramon A. Alvarez-Puebla. Fabrication of Plasmonic Supercrystals and Their SERS Enhancing Properties. ACS Omega 2020, 5 (40) , 25485-25492. https://doi.org/10.1021/acsomega.0c03412
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    14. Matthew T. Gole, Zhewen Yin, Michael Cai Wang, Wayne Lin, Ziran Zhou, Juyoung Leem, Satoshi Takekuma, Catherine J. Murphy, SungWoo Nam. Large scale self-assembly of plasmonic nanoparticles on deformed graphene templates. Scientific Reports 2021, 11 (1) https://doi.org/10.1038/s41598-021-91697-z
    15. Yi-Ting Cheng, Heng-Kwong Tsao, Yu-Jane Sheng. Interfacial assembly of nanorods: smectic alignment and multilayer stacking. Nanoscale 2021, 13 (33) , 14236-14244. https://doi.org/10.1039/D1NR03784F
    16. Ke Wang, Seong Hun Park, Jintao Zhu, Jung Kyu Kim, Lianbin Zhang, Gi‐Ra Yi. Self‐Assembled Colloidal Nanopatterns toward Unnatural Optical Meta‐Materials. Advanced Functional Materials 2021, 31 (12) https://doi.org/10.1002/adfm.202008246
    17. Satoshi Nakamura, Hideyuki Mitomo, Kuniharu Ijiro. Assembly and Active Control of Nanoparticles using Polymer Brushes as a Scaffold. Chemistry Letters 2021, 50 (2) , 361-370. https://doi.org/10.1246/cl.200767
    18. Merreta Noorenza Biutty, Maulida Zakia, Seong Il Yoo. Enhanced Photothermal Heating from One‐dimensional Assemblies of Au Nanoparticles Encapsulated by TiO 2 Shell. Bulletin of the Korean Chemical Society 2020, 41 (10) , 1033-1039. https://doi.org/10.1002/bkcs.12106
    19. J-C. Fernández-Toledano, C. Rigaut, M. Mastrangeli, J. De Coninck. Controlling the pinning time of a receding contact line under forced wetting conditions. Journal of Colloid and Interface Science 2020, 565 , 449-457. https://doi.org/10.1016/j.jcis.2020.01.054
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    21. Yoshiko Takenaka, Yoko Matsuzawa, Takuya Ohzono. Directed Assembly of Gold Nanorods by Microwrinkles. Chemistry Letters 2019, 48 (11) , 1292-1295. https://doi.org/10.1246/cl.190486
    22. Sung‐Hwan Lim, Min‐Jae Lee, Shin‐Hyun Kang, Jahar Dey, Aminah Umar, Sang‐Jo Lee, Sung‐Min Choi. Individually Silica‐Embedded Gold Nanorod Superlattice for High Thermal and Solvent Stability and Recyclable SERS Application. Advanced Materials Interfaces 2019, 6 (21) https://doi.org/10.1002/admi.201900986
    23. Heejung Kang, Sung‐Soo Kim, Seong Il Yoo, Byeong‐Hyeok Sohn. Dichroic Plasmon Superstructures of Au Nanorods over Macroscopic Areas via Directed Self‐Assemblies of Diblock Copolymers. Advanced Materials Interfaces 2019, 6 (22) https://doi.org/10.1002/admi.201901257
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    25. Chao Yu, Xuefeng Guo, Michelle Muzzio, Christopher T. Seto, Shouheng Sun. Self‐Assembly of Nanoparticles into Two‐Dimensional Arrays for Catalytic Applications. ChemPhysChem 2019, 20 (1) , 23-30. https://doi.org/10.1002/cphc.201800870
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    27. Walter R Caseri. Dichroic nanocomposites based on polymers and metallic particles: from biology to materials science. Polymer International 2018, 67 (1) , 46-54. https://doi.org/10.1002/pi.5455
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    ACS Applied Materials & Interfaces

    Cite this: ACS Appl. Mater. Interfaces 2017, 9, 30, 25513–25521
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acsami.7b06273
    Published July 7, 2017
    Copyright © 2017 American Chemical Society
    Request reuse permissions

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