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Phase-Controlled Synthesis of Cobalt Sulfides for Lithium Ion Batteries

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† CAS Key Laboratory of Materials for Energy Conversion, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, P.R. China
‡ Beijing National Laboratory for Molecular Sciences and State Key Laboratory of Rare Earth Materials Chemistry and Applications, College of Chemistry and Molecular Engineering, Peking University, Beijing 100871, P.R. China
§ College of Science, Northeastern University, Shenyang 110004, P.R.China
*E-mail: [email protected]; [email protected]. Fax: +86 21 5241 6360.
Cite this: ACS Appl. Mater. Interfaces 2012, 4, 8, 4246–4250
Publication Date (Web):July 25, 2012
https://doi.org/10.1021/am300951f
Copyright © 2012 American Chemical Society
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Abstract

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The polyhedral CoS2 with a narrow size distribution was synthesized by a facile solid-state assembly process in a sealed silica tube. The flux of potassium halide (KX; X = Cl, Br, I) plays a crucial role in the formation of polyhedrons and the size distribution. The S22– groups in CoS2 can be controllably withdrawn during heat treatment in air. The obtained phases and microstructures of CoS2, Co3S4, CoS, Co9S8, and CoO depended on heating temperature and time. These cobalt materials, successfully used as the electrodes of lithium ion batteries, possessed good cycling stability in lithium ion batteries. The discharge capacities of 929.1 and 835.2 mAh g–1 were obtained for CoS2 and CoS respectively, and 76% and 71% of the capacities remained after 10 cycles. High capacities and good cycle performance make them promising candidates for lithium ion batteries. The approach combining solid-state assembly and heat treatment provides a simple and versatile way to prepare various metal chalcogeides for energy storage applications.

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The heating procedure of the solid-state assembly (SSA) process, XRD and SEM analysis. This material is available free of charge via the Internet at http://pubs.acs.org.

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