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Recycling Rare Earth Elements from Industrial Wastewater with Flowerlike Nano-Mg(OH)2

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† State Key Laboratory of Structural Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002 P. R. China
‡ Key Laboratory of design and assembly of functional nanostructures, Chinese Academy of Sciences, Fuzhou, Fujian, 350002 China
§ Key Laboratory of Optoelectronic Materials Chemistry and Physical Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002 China
*E-mail: [email protected]. Tel/Fax: (+086)591-83705474.
Cite this: ACS Appl. Mater. Interfaces 2013, 5, 19, 9719–9725
Publication Date (Web):September 13, 2013
https://doi.org/10.1021/am4027967
Copyright © 2013 American Chemical Society
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Abstract

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Treatment of wastewater containing low-concentration yet highly-expensive rare earth elements (REEs) is one of the vital issues in the REEs separation and refining industry. In this work, the interaction and related mechanism between self-supported flowerlike nano-Mg(OH)2 and low-concentration REEs wastewater were investigated. More than 99% REEs were successfully taken up by nano-Mg(OH)2. Further analysis revealed that the REEs could be collected on the surface of Mg(OH)2 as metal hydroxide nanoparticles (<5 nm). An ion-exchange model was proposed as a critical factor for both guaranteeing the reaction speed and maintaining the self-supported structure of the materials. In addition, a method was developed to further separate the immobilized REEs and the residual magnesium hydroxide by varying the solution pH. In a pilot-scale experiment, the REEs from practical wastewater were immobilized effectively at a high flow rate. We anticipate this work can provide a good example for the recycling of valuable REEs in practical industrial applications.

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