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Catalytic Wet Oxidation of Lactose
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    Catalytic Wet Oxidation of Lactose
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    Department of Chemical Engineering, Michigan Technological University, 1400 Townsend Drive, Houghton Michigan 49931
    * Corresponding author. Tel: 1 906 487 1956 . Fax: 1 906 487 3213. E-mail: [email protected]
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    Industrial & Engineering Chemistry Research

    Cite this: Ind. Eng. Chem. Res. 2008, 47, 12, 4049–4055
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    https://doi.org/10.1021/ie701779u
    Published May 14, 2008
    Copyright © 2008 American Chemical Society

    Abstract

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    The catalytic wet oxidation of lactose to carbon dioxide/water and to a value-added product, lactobionic acid, has been demonstrated in a flow reactor. Lactose (milk sugar) is a low value byproduct of the dairy industry and makes up the largest part of the solids in cheese whey. Costs associated with cheese whey disposal are driving the need to develop alternative disposal methods. Pt/Al2O3, CeMn mixed-metal oxides, and Pt/CeMn catalysts have all been shown to effectively convert lactose to carbon dioxide and water at temperatures up to 443 K and pressures of 100 psig. Pt/CeMn demonstrated the lowest level of side-product formation. A BiPd/C catalyst was shown to convert essentially all lactose to lactobionic acid at similar temperature and pressure. Lactobionic acid selectivity was a strong function of oxygen concentration in the feed. The BiPd/C also produced a high yield of lactobionic acid at lower pH and higher temperatures than previously reported.

    Copyright © 2008 American Chemical Society

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    Cited By

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    This article is cited by 18 publications.

    1. Qinghua Lai, Michael D. Skoglund, Chen Zhang, Allen R. Morris, and Joseph H. Holles . Use of Hydrogen Chemisorption and Ethylene Hydrogenation as Predictors for Aqueous Phase Reforming of Lactose over Ni@Pt and Co@Pt Bimetallic Overlayer Catalysts. Energy & Fuels 2016, 30 (10) , 8587-8596. https://doi.org/10.1021/acs.energyfuels.6b01405
    2. Lidija Tetianec, Irina Bratkovskaja, Vida Časaitė, Vidutė Gurevičienė, Julija Razumienė, Jonita Stankevičiūtė, Rolandas Meškys, Marius Dagys, Audrius Laurynėnas. Efficient Bi-enzymatic synthesis of aldonic acids. Green Chemistry 2022, 24 (12) , 4902-4908. https://doi.org/10.1039/D2GC00823H
    3. D. E. Otter, S. Wu, D. N. De. S. Jayasinghe. Galacto-Oligosaccharides and Other Products Derived from Lactose. 2022, 125-228. https://doi.org/10.1007/978-3-030-92585-7_5
    4. Maryam Enteshari, Sergio I. Martínez-Monteagudo. One-Pot Synthesis of Lactose Derivatives from Whey Permeate. Foods 2020, 9 (6) , 784. https://doi.org/10.3390/foods9060784
    5. Arijit Nath, Balázs Verasztó, Somjyoti Basak, András Koris, Zoltán Kovács, Gyula Vatai. Synthesis of Lactose-Derived Nutraceuticals from Dairy Waste Whey—a Review. Food and Bioprocess Technology 2016, 9 (1) , 16-48. https://doi.org/10.1007/s11947-015-1572-2
    6. C. Vera, A. Illanes. Lactose-Derived Nondigestible Oligosaccharides and Other High Added-Value Products. 2016, 87-110. https://doi.org/10.1016/B978-0-12-802724-0.00003-2
    7. C. Guerrero, A. Illanes. Enzymatic Production of Other Lactose-Derived Prebiotic Candidates. 2016, 229-259. https://doi.org/10.1016/B978-0-12-802724-0.00006-8
    8. Micaela Pescuma, Graciela Font de Valdez, Fernanda Mozzi. Whey-derived valuable products obtained by microbial fermentation. Applied Microbiology and Biotechnology 2015, 99 (15) , 6183-6196. https://doi.org/10.1007/s00253-015-6766-z
    9. Francesco Arena. Multipurpose composite MnCeO x catalysts for environmental applications. Catal. Sci. Technol. 2014, 4 (7) , 1890-1898. https://doi.org/10.1039/C4CY00022F
    10. Saúl Alonso, Manuel Rendueles, Mario Díaz. Bio-production of lactobionic acid: Current status, applications and future prospects. Biotechnology Advances 2013, 31 (8) , 1275-1291. https://doi.org/10.1016/j.biotechadv.2013.04.010
    11. Saúl Alonso, Manuel Rendueles, Mario Díaz. Feeding strategies for enhanced lactobionic acid production from whey by Pseudomonas taetrolens. Bioresource Technology 2013, 134 , 134-142. https://doi.org/10.1016/j.biortech.2013.01.145
    12. Luis-Felipe Gutiérrez, Safia Hamoudi, Khaled Belkacemi. Lactobionic acid: A high value-added lactose derivative for food and pharmaceutical applications. International Dairy Journal 2012, 26 (2) , 103-111. https://doi.org/10.1016/j.idairyj.2012.05.003
    13. Luis-Felipe Gutiérrez, Safia Hamoudi, Khaled Belkacemi. Effective gold catalyst supported on mesoporous silica decorated by ceria for the synthesis of high value lactobionic acid. Applied Catalysis A: General 2012, 425-426 , 213-223. https://doi.org/10.1016/j.apcata.2012.03.025
    14. Klara Piotrowska, Mirosław Imbierowicz, Andrzej Chacuk. Wet Oxidation of Dairy Sewage. Ecological Chemistry and Engineering S 2012, 19 (1) , 29-38. https://doi.org/10.2478/v10216-011-0003-1
    15. Saúl Alonso, Manuel Rendueles, Mario Díaz. Efficient lactobionic acid production from whey by Pseudomonas taetrolens under pH-shift conditions. Bioresource Technology 2011, 102 (20) , 9730-9736. https://doi.org/10.1016/j.biortech.2011.07.089
    16. Luis-Felipe Gutierrez, Safia Hamoudi, Khaled Belkacemi. Selective production of lactobionic acid by aerobic oxidation of lactose over gold crystallites supported on mesoporous silica. Applied Catalysis A: General 2011, 402 (1-2) , 94-103. https://doi.org/10.1016/j.apcata.2011.05.034
    17. Maria J. Climent, Avelino Corma, Sara Iborra. Converting carbohydrates to bulk chemicals and fine chemicals over heterogeneous catalysts. Green Chemistry 2011, 13 (3) , 520. https://doi.org/10.1039/c0gc00639d
    18. Päivi Mäki-Arvela, Anton V. Tokarev, Elena V. Murzina, Betiana Campo, Teemu Heikkilä, Jenny-Maria Brozinski, Dorit Wolf, Dmitry Yu. Murzin. Kinetics of lactose and rhamnose oxidation over supported metal catalysts. Physical Chemistry Chemical Physics 2011, 13 (20) , 9268. https://doi.org/10.1039/c1cp20081j

    Industrial & Engineering Chemistry Research

    Cite this: Ind. Eng. Chem. Res. 2008, 47, 12, 4049–4055
    Click to copy citationCitation copied!
    https://doi.org/10.1021/ie701779u
    Published May 14, 2008
    Copyright © 2008 American Chemical Society

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