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Composite Recycling with Biocatalytic Thermoset Reforming
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    Composite Recycling with Biocatalytic Thermoset Reforming
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    • Clarissa Olivar
      Clarissa Olivar
      Department of Chemistry, Donald P. and Katherine B. Loker Hydrocarbon Institute, and Wrigley Institute for Environment and Sustainability, University of Southern California, Los Angeles, California 90089, United States
    • Zehan Yu
      Zehan Yu
      Department of Chemical Engineering & Materials Science and M.C. Gill Composites Center, University of Southern California, Los Angeles, California 90089, United States
      More by Zehan Yu
    • Ben Miller
      Ben Miller
      Department of Chemistry, Donald P. and Katherine B. Loker Hydrocarbon Institute, and Wrigley Institute for Environment and Sustainability, University of Southern California, Los Angeles, California 90089, United States
      Department of Pharmacology & Pharmaceutical Sciences, University of Southern California, Los Angeles, California 90089, United States
      More by Ben Miller
    • Maria Tangalos
      Maria Tangalos
      Department of Chemistry, Donald P. and Katherine B. Loker Hydrocarbon Institute, and Wrigley Institute for Environment and Sustainability, University of Southern California, Los Angeles, California 90089, United States
      Department of Pharmacology & Pharmaceutical Sciences, University of Southern California, Los Angeles, California 90089, United States
    • Cory B. Jenkinson
      Cory B. Jenkinson
      Department of Molecular Biosciences, University of Kansas, Lawrence, Kansas 66045, United States
    • Steven R. Nutt
      Steven R. Nutt
      Department of Chemical Engineering & Materials Science and M.C. Gill Composites Center, University of Southern California, Los Angeles, California 90089, United States
    • Berl R. Oakley
      Berl R. Oakley
      Department of Molecular Biosciences, University of Kansas, Lawrence, Kansas 66045, United States
    • Clay C. C. Wang*
      Clay C. C. Wang
      Department of Chemistry, Donald P. and Katherine B. Loker Hydrocarbon Institute, and Wrigley Institute for Environment and Sustainability, University of Southern California, Los Angeles, California 90089, United States
      Department of Pharmacology & Pharmaceutical Sciences, University of Southern California, Los Angeles, California 90089, United States
      *Email: [email protected]
    • Travis J. Williams*
      Travis J. Williams
      Department of Chemistry, Donald P. and Katherine B. Loker Hydrocarbon Institute, and Wrigley Institute for Environment and Sustainability, University of Southern California, Los Angeles, California 90089, United States
      *Email: [email protected]
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    Journal of the American Chemical Society

    Cite this: J. Am. Chem. Soc. 2024, 146, 44, 30004–30008
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    https://doi.org/10.1021/jacs.4c10838
    Published October 24, 2024
    Copyright © 2024 American Chemical Society

    Abstract

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    Carbon fiber reinforced polymers (CFRPs, or composites) are increasingly replacing traditional manufacturing materials used in the automobile, aerospace, and energy sectors. With this shift, it is vital to develop end-of-life processes for CFRPs that retain the value of both the carbon fibers and the polymer matrix. Here we demonstrate a strategy to upcycle pre- and postconsumer polystyrene-containing CFRPs, cross-linked with unsaturated polyesters or vinyl esters, to benzoic acid. The thermoset matrix is upgraded via biocatalysis utilizing an engineered strain of the filamentous fungus Aspergillus nidulans, which gives access to valuable secondary metabolites in high yields, exemplified here by (2Z,4Z,6E)-octa-2,4,6-trienoic acid. Reactions are engineered to preserve the carbon fibers with much of their sizing so that the isolated carbon fiber plies are manufactured into new composite coupons that exhibit mechanical properties comparable to those of virgin manufacturing substrates. In sum, this represents the first system to reclaim a high value from both the fiber fabric and polymer matrix of a CFRP.

    Copyright © 2024 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/jacs.4c10838.

    • Procedures for optimization of reaction conditions, compound and recovered fiber purification, media recipes and fungal metabolism, Aspergillus nidulans strain engineering, NMR spectra and chemical shift data, IR spectra, UV–vis spectrum, XPS spectra, and SEM images (PDF)

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    Journal of the American Chemical Society

    Cite this: J. Am. Chem. Soc. 2024, 146, 44, 30004–30008
    Click to copy citationCitation copied!
    https://doi.org/10.1021/jacs.4c10838
    Published October 24, 2024
    Copyright © 2024 American Chemical Society

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