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Efficient Light-Driven Ion Pumping for Deep Desalination via the Vertical Gradient Protonation of Covalent Organic Framework Membranes
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    Efficient Light-Driven Ion Pumping for Deep Desalination via the Vertical Gradient Protonation of Covalent Organic Framework Membranes
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    • Weipeng Xian
      Weipeng Xian
      Zhejiang Provincial Key Laboratory of Advanced Chemical Engineering Manufacture Technology, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310058, China
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    • Xiaoyi Xu
      Xiaoyi Xu
      State Key Laboratory of Silicon and Advanced Semiconductor Materials, Department of Polymer Science and Engineering, Zhejiang University, Hangzhou 310058, China
      More by Xiaoyi Xu
    • Yongxin Ge
      Yongxin Ge
      State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China
      University of Chinese Academy of Sciences, Beijing 100049, China
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    • Zhiwei Xing
      Zhiwei Xing
      Zhejiang Provincial Key Laboratory of Advanced Chemical Engineering Manufacture Technology, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310058, China
      More by Zhiwei Xing
    • Zhuozhi Lai
      Zhuozhi Lai
      Zhejiang Provincial Key Laboratory of Advanced Chemical Engineering Manufacture Technology, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310058, China
      More by Zhuozhi Lai
    • Qing-Wei Meng
      Qing-Wei Meng
      Zhejiang Provincial Key Laboratory of Advanced Chemical Engineering Manufacture Technology, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310058, China
    • Zhifeng Dai
      Zhifeng Dai
      Key Laboratory of Surface & Interface Science of Polymer Materials of Zhejiang Province, School of Chemistry and Chemical Engineering, Zhejiang Sci-Tech University, Hangzhou 310018, China
      Longgang Institute of Zhejiang Sci-Tech University, Wenzhou 325802, China
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    • Sai Wang*
      Sai Wang
      Hangzhou Institute of Advanced Studies, Zhejiang Normal University, Hangzhou 310015, China
      *Email: [email protected]
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    • Ruotian Chen
      Ruotian Chen
      State Key Laboratory of Catalysis, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China
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    • Ning Huang
      Ning Huang
      State Key Laboratory of Silicon and Advanced Semiconductor Materials, Department of Polymer Science and Engineering, Zhejiang University, Hangzhou 310058, China
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    • Shengqian Ma
      Shengqian Ma
      Department of Chemistry, University of North Texas, 1508 W Mulberry St, Denton, Texas 76201, United States
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    • Qi Sun*
      Qi Sun
      Zhejiang Provincial Key Laboratory of Advanced Chemical Engineering Manufacture Technology, College of Chemical and Biological Engineering, Zhejiang University, Hangzhou 310058, China
      *Email: [email protected]
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    Journal of the American Chemical Society

    Cite this: J. Am. Chem. Soc. 2024, 146, 49, 33973–33982
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    https://doi.org/10.1021/jacs.4c12829
    Published November 28, 2024
    Copyright © 2024 American Chemical Society

    Abstract

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    Traditional desalination methods face criticism due to high energy requirements and inadequate trace ion removal, whereas natural light-driven ion pumps offer superior efficiency. Current synthetic systems are constrained by short exciton lifetimes, which limit their ability to generate sufficient electric fields for effective ion pumping. We introduce an innovative approach utilizing covalent-organic framework membranes that enhance light absorption and reduce charge recombination through vertical gradient protonation of imine linkages during acid-catalyzed liquid–liquid interfacial polymerization. This technique creates intralayer and interlayer heterojunctions, facilitating interlayer hybridization and establishing a robust built-in electric field under illumination. These improvements enable the membranes to achieve remarkable ion transport across extreme concentration gradients (2000:1), with a transport rate of approximately 3.2 × 1012 ions per second per square centimeter and reduce ion concentrations to parts per billion. This performance significantly surpasses that of conventional reverse osmosis systems, representing a major advancement in solar-powered desalination technology by substantially reducing energy consumption and secondary waste.

    Copyright © 2024 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/jacs.4c12829.

    • Experimental procedures, materials, characterization, ion-pumping measurement, light-responsive transmembrane ion transport evaluation, ion rectification measurement, DFT calculations, membrane digital photographs, membrane wettability assessment, SEM image, HR-TEM image, ATR-FTIR spectra, XPS spectra, N2 sorption isotherms, XRD patterns, UV–vis spectra and corresponding Tauc plots, UPS spectra, KPFM images, SPV spectra, Xenon lamp spectrum, and table comparing ion pumping systems (PDF)

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    Journal of the American Chemical Society

    Cite this: J. Am. Chem. Soc. 2024, 146, 49, 33973–33982
    Click to copy citationCitation copied!
    https://doi.org/10.1021/jacs.4c12829
    Published November 28, 2024
    Copyright © 2024 American Chemical Society

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