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Pb17O8Cl18: A Promising IR Nonlinear Optical Material with Large Laser Damage Threshold Synthesized in an Open System

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† Key Laboratory of Functional Materials and Devices for Special Environments, Xinjiang Technical Institute of Physics & Chemistry, Chinese Academy of Sciences; Xinjiang Key Laboratory of Electronic Information Materials and Devices, 40-1 South Beijing Road, Urumqi 830011, China
‡ University of Chinese Academy of Sciences, Beijing 100049, China
§ Department of Chemistry, Northwestern University, 2145 Sheridan Road, Evanston, Illinois 60208-3113, United States
*[email protected]
*[email protected]
*[email protected]
Cite this: J. Am. Chem. Soc. 2015, 137, 26, 8360–8363
Publication Date (Web):June 29, 2015
https://doi.org/10.1021/jacs.5b03986
Copyright © 2015 American Chemical Society
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Mid-IR nonlinear optical (NLO) materials are of great importance in modern laser frequency conversion technology and optical parametric oscillator processes. However, the commercially available IR NLO crystals (e.g., AgGaQ2 (Q = S, Se) and ZnGeP2) suffer from two obstacles, low laser damage thresholds (LDTs) and the difficulty of obtaining high-quality crystals, both of which seriously hinder their applications. The introduction of Cl, an element with a large electronegativity, and Pb, a relatively heavy element to promote the optical properties, affords an oxide-based IR NLO material, Pb17O8Cl18 (POC). High-quality POC single crystals with sizes of up to 7 mm × 2 mm × 2 mm have been grown in an open system. Additionally, POC exhibits a large LDT of 408 MW/cm2, 12.8 times that of AgGaS2. POC also exhibits an excellent second harmonic generation response: 2 times that of AgGaS2, the benchmark IR NLO crystal at 2090 nm, and 4 times that of KDP, the standard UV NLO crystal at 1064 nm. Thus, we believe that POC is a promising IR NLO material.

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Crystallographic data (CIF), experimental methods, and additional tables and figures. The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/jacs.5b03986.

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