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Visible-Light-Driven Photocatalytic CO2 Reduction by a Ni(II) Complex Bearing a Bioinspired Tetradentate Ligand for Selective CO Production

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† Department of Chemistry, Faculty of Pure and Applied Sciences, University of Tsukuba and CREST (JST), 1-1-1 Tennoudai, Tsukuba, Ibaraki 305-8571, Japan
‡ Interdisciplinary Research Center for Catalytic Chemistry, National Institute of Advanced Industrial Science and Technology (AIST), Tsukuba, Ibaraki 305-8565, Japan
*[email protected]
Cite this: J. Am. Chem. Soc. 2017, 139, 19, 6538–6541
Publication Date (Web):April 28, 2017
https://doi.org/10.1021/jacs.7b01956
Copyright © 2017 American Chemical Society
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Abstract

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A Ni(II) complex bearing an S2N2-type tetradentate ligand inspired by the active site of carbon monoxide dehydrogenase was found to selectively catalyze CO2 reduction to produce CO in a photocatalytic system using [Ru(bpy)3]2+ (bpy = 2,2′-bipyridine) as a photosensitizer and 1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole (BIH) as an electron donor. The Ni(II) complex shows a high turnover number over 700 with high CO selectivity of >99% and quantum yield of 1.42% in the photocatalytic system.

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The Supporting Information is available free of charge on the ACS Publications website at DOI: 10.1021/jacs.7b01956.

  • Experimental details and analytical data, including Figures S1–S16 and Tables S1 and S2 (PDF)

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