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A simplified high-performance liquid chromatographic residue procedure for the determination of glyphosate herbicide and (aminomethyl)phosphonic acid in fruits and vegetables employing postcolumn fluorogenic labeling

Cite this: J. Agric. Food Chem. 1983, 31, 1, 69–72
Publication Date (Print):January 1, 1983
https://doi.org/10.1021/jf00115a018
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    This article is cited by 53 publications.

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    2. Kenta Ishii, Akito Takeuchi, Osamu Nishinoiri, Ginji Endo, Mariko Ono-Ogasawara. Development of a method to determine workers' personal exposure levels to glyphosate. Journal of Occupational Health 2022, 64 (1) https://doi.org/10.1002/1348-9585.12345
    3. Bhim Bali Prasad, Darshika Jauhari, Mahavir Prasad Tiwari. Doubly imprinted polymer nanofilm-modified electrochemical sensor for ultra-trace simultaneous analysis of glyphosate and glufosinate. Biosensors and Bioelectronics 2014, 59 , 81-88. https://doi.org/10.1016/j.bios.2014.03.019
    4. A.M. Botero-Coy, M. Ibáñez, J.V. Sancho, F. Hernández. Direct liquid chromatography–tandem mass spectrometry determination of underivatized glyphosate in rice, maize and soybean. Journal of Chromatography A 2013, 1313 , 157-165. https://doi.org/10.1016/j.chroma.2013.07.037
    5. Xuan Wei, Xiaotong Gao, Lei Zhao, Xianglu Peng, Lei Zhou, Jing Wang, Qiaosheng Pu. Fast and interference-free determination of glyphosate and glufosinate residues through electrophoresis in disposable microfluidic chips. Journal of Chromatography A 2013, 1281 , 148-154. https://doi.org/10.1016/j.chroma.2013.01.039
    6. Ming-Xue Chen, Zhao-Yun Cao, Yan Jiang, Zhi-Wei Zhu. Direct determination of glyphosate and its major metabolite, aminomethylphosphonic acid, in fruits and vegetables by mixed-mode hydrophilic interaction/weak anion-exchange liquid chromatography coupled with electrospray tandem mass spectrometry. Journal of Chromatography A 2013, 1272 , 90-99. https://doi.org/10.1016/j.chroma.2012.11.069
    7. Pavel Jandera, Peter Lembke. Liquid Chromatography, 2. Methods, Programmed and Coupling Techniques. 2011https://doi.org/10.1002/14356007.o15_o01
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    9. Chihiro YOSHIOKA, Hiroshi SUZUKI, Masako ISHIKAWA, Takefumi YOKOKURA, Toshihiro SHIRASAKI. Determination of Glyphosate and Its Major Metabolite Aminomethylphosphonic Acid in River Water and Tap Water by High-Performance Liquid Chromatography with Postcolumn Derivatization Method. BUNSEKI KAGAKU 2006, 55 (3) , 177-184. https://doi.org/10.2116/bunsekikagaku.55.177
    10. M.P. García de Llasera, L. Gómez-Almaraz, L.E. Vera-Avila, A. Peña-Alvarez. Matrix solid-phase dispersion extraction and determination by high-performance liquid chromatography with fluorescence detection of residues of glyphosate and aminomethylphosphonic acid in tomato fruit. Journal of Chromatography A 2005, 1093 (1-2) , 139-146. https://doi.org/10.1016/j.chroma.2005.07.063
    11. J.L. Tadeo, C. Sánchez-Brunete, B. Albero. Detecting herbicide residues. 2004, 386-410. https://doi.org/10.1533/9781855739109.3.386
    12. K. Granby, S. Johannesen, M. Vahl. Analysis of glyphosate residues in cereals using liquid chromatography-mass spectrometry (LC-MS/MS). Food Additives and Contaminants 2003, 20 (8) , 692-698. https://doi.org/10.1080/0265203031000109477
    13. Kit Granby, Martin Vahl. Investigation of the herbicide glyphosate and the plant growth regulators chlormequat and mepiquat in cereals produced in Denmark. Food Additives and Contaminants 2001, 18 (10) , 898-905. https://doi.org/10.1080/02652030119594
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    18. Kunihiko TAKAHASHI, Masakazu HORIE, Nobuji AOBA. Analysis of Glyphosate and Its Metabolite, Aminomethylphosphonic Acid, in Agricultural Products by HPLC.. Journal of the Food Hygienic Society of Japan (Shokuhin Eiseigaku Zasshi) 2001, 42 (5) , 304-308. https://doi.org/10.3358/shokueishi.42.304
    19. Maarten Honing. Carbamate and Carbamoyloxime Insecticides: Single‐Class, Multiresidue Analysis of. 2000https://doi.org/10.1002/9780470027318.a1704
    20. Elisabet Börjesson, Lennart Torstensson. New methods for determination of glyphosate and (aminomethyl)phosphonic acid in water and soil. Journal of Chromatography A 2000, 886 (1-2) , 207-216. https://doi.org/10.1016/S0021-9673(00)00514-8
    21. J.L Tadeo, C Sánchez-Brunete, R.A Pérez, M.D Fernández. Analysis of herbicide residues in cereals, fruits and vegetables. Journal of Chromatography A 2000, 882 (1-2) , 175-191. https://doi.org/10.1016/S0021-9673(00)00103-5
    22. Ichiro TAKANO, Toshihiro NAGAYAMA, Maki KOBAYASHI, Masako ITO, Yasuhiro TAMURA, Chieko TAKADA, Naoko KIMURA, Kyoko KITAYAMA, Kazuo YASUDA. A Simplified HPLC Procedure for the Determination of Glyphosate in Soybeans Employing Postcolumn Fluorescence Labeling.. Journal of the Food Hygienic Society of Japan (Shokuhin Eiseigaku Zasshi) 2000, 41 (4) , 242-245. https://doi.org/10.3358/shokueishi.41.242
    23. E.A. Hogendoorn, F.M. Ossendrijver, E. Dijkman, R.A. Baumann. Rapid determination of glyphosate in cereal samples by means of pre-column derivatisation with 9-fluorenylmethyl chloroformate and coupled-column liquid chromatography with fluorescence detection. Journal of Chromatography A 1999, 833 (1) , 67-73. https://doi.org/10.1016/S0021-9673(98)01055-3
    24. E Mallat, D Barceló. Analysis and degradation study of glyphosate and of aminomethylphosphonic acid in natural waters by means of polymeric and ion-exchange solid-phase extraction columns followed by ion chromatography–post-column derivatization with fluorescence detection. Journal of Chromatography A 1998, 823 (1-2) , 129-136. https://doi.org/10.1016/S0021-9673(98)00362-8
    25. J. Klinger, M. Lang, F. Sacher, H.-J. Brauch, D. Maier, E. Worch. Formation of Glyphosate and AMPA During Ozonation of Waters Containing Ethylenediaminetetra(methylenephosphonic acid). Ozone: Science & Engineering 1998, 20 (2) , 99-110. https://doi.org/10.1080/01919519808547279
    26. K. M. S. Sundaram, J. Curry. A Comparison of UV and Fluorescence Detectors in the Liquid Chromatographic Analysis of Glyphosate Deposits After Post-Column Derivatization. Journal of Liquid Chromatography & Related Technologies 1997, 20 (4) , 511-524. https://doi.org/10.1080/10826079708010941
    27. J.V Sancho, F Hernández, F.J López, E.A Hogendoorn, E Dijkman. Rapid determination of glufosinate, glyphosate and aminomethylphosphonic acid in environmental water samples using precolumn fluorogenic labeling and coupled-column liquid chromatography. Journal of Chromatography A 1996, 737 (1) , 75-83. https://doi.org/10.1016/0021-9673(96)00071-4
    28. Hiroyuki Kataoka, Sunhi Ryu, Norihisa Sakiyama, Masami Makita. Simple and rapid determination of the herbicides glyphosate and glufosinate in river water, soil and carrot samples by gas chromatography with flame photometric detection. Journal of Chromatography A 1996, 726 (1-2) , 253-258. https://doi.org/10.1016/0021-9673(95)01071-8
    29. J. V. Sancho, C. Hidalgo, F. Hernández, F. J. López, E. Dijkman, E. A. Hogendoorn. Rapid Determination of Glyphosate Residues and Its Main Metabolite Ampa in Soil Samples by Liquid Chromatography. International Journal of Environmental Analytical Chemistry 1996, 62 (1) , 53-63. https://doi.org/10.1080/03067319608027052
    30. M. Honing, D. Barceló, B.L.M. van Baar, U.A.Th. Brinkman. 22. Sample handling and determination of carbamate pesticides and their transformation products in various matrices. 1995, 535-562. https://doi.org/10.1016/S0167-9244(06)80023-5
    31. Brian D. McGarvey. Derivatization reactions applicable to pesticide determination by high-performance liquid chromatography. Journal of Chromatography B: Biomedical Sciences and Applications 1994, 659 (1-2) , 243-257. https://doi.org/10.1016/0378-4347(94)80122-3
    32. J.V. Sancho, F.J. López, F. Hernández, E.A. Hogendoorn, P. van Zoonen. Rapid determination of glufosinate in environmental water samples using 9-fluorenylmethoxycarbonyl precolumn derivatization, large-volume injection and coupled-column liquid chromatography. Journal of Chromatography A 1994, 678 (1) , 59-67. https://doi.org/10.1016/0021-9673(94)87074-8
    33. Kelvin P. Spann, Phillip A. Hargreaves. The determination of glyphosate in soils with moderate to high clay content. Pesticide Science 1994, 40 (1) , 41-48. https://doi.org/10.1002/ps.2780400108
    34. N. Tsunoda. Simultaneous determination of the herbicides glyphosate, glufosinate and bialaphos and their metabolites by capillary gas chromatography—ion-trap mass spectrometry. Journal of Chromatography A 1993, 637 (2) , 167-173. https://doi.org/10.1016/0021-9673(93)83209-B
    35. János Répási. Selective complexometric determination of glyphosate and related compounds. Pesticide Science 1993, 39 (4) , 287-292. https://doi.org/10.1002/ps.2780390406
    36. Ch.E. Kientz, A. Verweij, G.J. de Jong, U.A. Th. Brinkman. Flame-based thermionic detection coupled on-line with microcolumn liquid chromatography. Journal of Chromatography A 1992, 626 (1) , 59-69. https://doi.org/10.1016/0021-9673(92)85329-R
    37. Michael J. Lovdahl, Donald J. Pietrzyk. Liquid chromatography and postcolumn indirect detection of glyphosate. Journal of Chromatography A 1992, 602 (1-2) , 197-204. https://doi.org/10.1016/0021-9673(92)80081-5
    38. O Samuel, J-G Guillot. The Efficiency of Cold Water Machine Washing in Removing Glyphosate from Work Garments. 1992, 811-817. https://doi.org/10.1520/STP19208S
    39. Yuk Y. Wigfield, Monique Lanouette. A modified clean‐up for the determination of glyphosate and its metabolite residues in lentils using high pressure liquid chromatography and post‐column fluorogenic labelling. Pesticide Science 1991, 33 (4) , 491-498. https://doi.org/10.1002/ps.2780330411
    40. Satohsi Kawai, Bunji Uno, Masafumi Tomita. Determination of glyphosate and its major metabolite aminomethylphosphonic acid by high-performance liquid chromatography after derivatization with p-toluenesulphonyl chloride. Journal of Chromatography A 1991, 540 , 411-415. https://doi.org/10.1016/S0021-9673(01)88832-4
    41. Alan Ronald Talbot, Mon-Han Shiaw, Jinn-Sheng Huang, Shu-Fen Yang, Tein-Shong Goo, Shur-Hueih Wang, Chao-Liang Chen, Thomas Richard Sanford. Acute Poisoning with a Glyphosate-Surfactant Herbicide ('Roundup'): A Review of 93 Cases. Human & Experimental Toxicology 1991, 10 (1) , 1-8. https://doi.org/10.1177/096032719101000101
    42. Yuk Y. Wigfield, Monique Lanouette. Simplified liquid chromatographic determination of glyphosate and metabolite residues in environmental water using post-column fluorogenic labelling. Analytica Chimica Acta 1990, 233 , 311-314. https://doi.org/10.1016/S0003-2670(00)83495-9
    43. S.K. Konar, D.N. Roy. Method for the determination of residues of the herbicide glyphosate and its principal metabolite, aminomethylphosphonic acid, in plant materials by nitrogen-selective gas chromatography. Analytica Chimica Acta 1990, 229 , 277-280. https://doi.org/10.1016/S0003-2670(00)85139-9
    44. H.A. Powell, N.W. Kerby, P. Rowell. High-performance liquid chromatographic determination of the herbicide glyphosate and its metabolite (aminomethyl)phosphonic acid and their extraction from cyanobacteria. Journal of Chromatography A 1990, 502 , 201-207. https://doi.org/10.1016/S0021-9673(01)89580-7
    45. R.J. Demchak, J.G. MacConnell. Normal-phase chromatography and post-column colorimetric detection of abamectin-8,9-oxide. Journal of Chromatography A 1990, 511 , 353-358. https://doi.org/10.1016/S0021-9673(01)93298-4
    46. D. Barceló. A review of liquid chromatography in environmental pesticide analysis. Chromatographia 1988, 25 (10) , 928-936. https://doi.org/10.1007/BF02311434
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    48. R. Weinberger, R.A. Femia. Chapter 8 Commercial Aspects of Post-Column Reaction Detectors for Liquid Chromatography. 1988, 395-435. https://doi.org/10.1016/S0301-4770(08)60384-X
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    50. Ludmila Křivánková, Petr Boček. Analytical control of the production of herbicides and growth regulators glyphosate and glyphosine by capillary isotachophoresis. ELECTROPHORESIS 1986, 7 (2) , 100-103. https://doi.org/10.1002/elps.1150070210
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