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One-flask preparation of analytically pure dipotassium tetracarbonylferrate

Cite this: J. Org. Chem. 1978, 43, 11, 2279–2280
Publication Date (Print):May 1, 1978
https://doi.org/10.1021/jo00405a041
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    3. Takako Muraoka, Hideaki Motohashi, Hiroki Tomura, and Keiji Ueno . Photoinduced Formal Gallylene Transfer from Gallium-Bridged Dimetallic Complexes to 16-Electron Metal Fragments. Organometallics 2013, 32 (2) , 643-648. https://doi.org/10.1021/om301148y
    4. Hisako Hashimoto,, Katsunori Suzuki,, Wataru Setaka,, Chizuko Kabuto, and, Mitsuo Kira. Iron Complexes of (E)- and (Z)-1,2-Dichlorodisilenes. Journal of the American Chemical Society 2004, 126 (42) , 13628-13629. https://doi.org/10.1021/ja048100i
    5. John E. Ellis. Metal Carbonyl Anions:  from [Fe(CO)4]2- to [Hf(CO)6]2- and Beyond. Organometallics 2003, 22 (17) , 3322-3338. https://doi.org/10.1021/om030105l
    6. Alan H. Cowley,, Viviana Lomelí, and, Andreas Voigt. Synthesis and Characterization of a Terminal Borylene (Boranediyl) Complex. Journal of the American Chemical Society 1998, 120 (25) , 6401-6402. https://doi.org/10.1021/ja9806433
    7. Jian Xu, Sudip Pan, Shenglai Yao, Gernot Frenking, Matthias Driess. The Heaviest Bottleable Metallylone: Synthesis of a Monatomic, Zero‐Valent Lead Complex (“Plumbylone”). Angewandte Chemie 2022, 134 (38) https://doi.org/10.1002/ange.202209442
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    9. Rajkumar Jana, Subrata Chakraborty, Olivier Blacque, Heinz Berke. Manganese and Rhenium Formyl Complexes of Diphosphanylborane Ligands: Stabilization of the Formyl Unit from Intramolecular B–O Bond Formation. European Journal of Inorganic Chemistry 2013, 2013 (26) , 4574-4584. https://doi.org/10.1002/ejic.201300482
    10. . Carbonylation. 2012, 117-152. https://doi.org/10.1002/9781119942863.ch4
    11. Manuel Alcarazo, Christian W. Lehmann, Anakuthil Anoop, Walter Thiel, Alois Fürstner. Coordination chemistry at carbon. Nature Chemistry 2009, 1 (4) , 295-301. https://doi.org/10.1038/nchem.248
    12. Benoît Blank, Miriam Colling-Hendelkens, Carsten Kollann, Krzysztof Radacki, Daniela Rais, Katharina Uttinger, George R. Whittell, Holger Braunschweig. Aminoborylene Complexes of Group 6 Elements and Iron: A Synthetic, Structural, and Quantum Chemical Study. Chemistry - A European Journal 2007, 13 (17) , 4770-4781. https://doi.org/10.1002/chem.200601520
    13. Keiji Ueno, Masakazu Hirotsu, Naoki Hatori. Synthesis and structure of a dmpe-substituted dinuclear complex bridged by a substituent-free gallium atom: Electronic effect of metal fragment on the iron–gallium bonding. Journal of Organometallic Chemistry 2007, 692 (1-3) , 88-92. https://doi.org/10.1016/j.jorganchem.2006.08.052
    14. Tse-Lok Ho, Mary Fieser, Louis Fieser. Dipotassium Tetracarbonylferrate. 2006https://doi.org/10.1002/9780471264194.fos04849
    15. Robert D. Pike. Disodium Tetracarbonylferrate(−II). 2001https://doi.org/10.1002/047084289X.rd465
    16. Holger Fölsing, Oliver Segnitz, Ursula Bossek, Klaus Merz, Manuela Winter, Roland A Fischer. Synthesis and structure of adduct stabilized Group III metal transition metal carbonyl complexes: new examples for FeGa, FeIn, WAl, CrAl and CrGa bonds. Journal of Organometallic Chemistry 2000, 606 (2) , 132-140. https://doi.org/10.1016/S0022-328X(00)00279-5
    17. Yu-Sen Chen, John E. Ellis. Highly reduced organometallics 52. Synthesis and chemistry of tricarbonylnitrosylmanganate(2−), [Mn(CO)3(NO)]2−. Inorganica Chimica Acta 2000, 300-302 , 675-682. https://doi.org/10.1016/S0020-1693(99)00546-0
    18. Jurij Weiss, Dana Stetzkamp, Bernhard Nuber, Roland A. Fischer, Christian Boehme, Gernot Frenking. [(η 5 ‐C 5 Me 5 )AlFe(CO) 4 ]—Synthesis, Structure, and Bonding. Angewandte Chemie International Edition in English 1997, 36 (1-2) , 70-72. https://doi.org/10.1002/anie.199700701
    19. Jurij Weiß, Dana Stetzkamp, Bernhard Nuber, Roland A. Fischer, Christian Boehme, Gernot Frenking. [(η 5 ‐Cp*)AlFe(CO) 4 ] – Synthese, Struktur, Bindungsverhältnisse. Angewandte Chemie 1997, 109 (1-2) , 95-97. https://doi.org/10.1002/ange.19971090127
    20. Roland A. Fischer, Markus M. Schulte, Thomas Priermeier. The first volatile Di(organogallio) transition metal carbonylates: cis-(CO)4Fe{Ga[(CH2)3NMe2](R)}2 (RtBu or C6H5), Precursors for Gallium rich thin FeGa alloy films. Journal of Organometallic Chemistry 1995, 493 (1-2) , 139-142. https://doi.org/10.1016/0022-328X(94)05349-G
    21. Roderick W. Bates. Transition Metal Carbonyl Complexes. 1995, 349-386. https://doi.org/10.1016/B978-008046519-7.00115-5
    22. Anne Baby, Jean-Jacques Brunet, Fadjai B. Kindela, Denis Neibecker. Convenient Preparation and Use of Potassium Tetracarbonylferrate, K 2 [Fe(CO) 4 ], an Easy-to-Handle Analogue of the Collman Reagent. Synthetic Communications 1994, 24 (20) , 2827-2834. https://doi.org/10.1080/00397919408010602
    23. Masakazu Yamashita, Takahiro Ohishi. Dimerization of aldehydes to carboxylic esters catalyzed by K2[Fe(CO)4]-crown ether system. Applied Organometallic Chemistry 1993, 7 (5) , 357-361. https://doi.org/10.1002/aoc.590070510
    24. Masakazu Yamashita, Haruyoshi Tashika, Masaya Uchida. Hydroacylation of Alkyl Vinyl Ketones and Acrylic Esters Using Organotetracarbonylferrates. Synthesis of 1,4-Dicarbonyl Compounds. Bulletin of the Chemical Society of Japan 1992, 65 (5) , 1257-1261. https://doi.org/10.1246/bcsj.65.1257
    25. Marcetta Y. Darensbourg, Carlton E. Ash, Larry W. Arndt, Christopher P. Janzen, Kay A. Youngdahl, Yong K. Park. Reactions of anionic transition metal carbonyl hydrides with electrophilic metal carbonyls: Nucleophilic addition (hydride transfer) vs. electron transfer mechanisms. Journal of Organometallic Chemistry 1990, 383 (1-3) , 191-199. https://doi.org/10.1016/0022-328X(90)85131-H
    26. John E. Ellis. Highly Reduced Metal Carbonyl Anions: Synthesis, Characterization, and Chemical Properties. 1990, 1-51. https://doi.org/10.1016/S0065-3055(08)60508-0
    27. Masakazu Yamashita, Masaya Uchida, Haruyoshi Tashika, Rikisaku Suemitsu. Synthesis of Five-Membered Cyclic Ketones Using Potassium Tetracarbonylferrate(2—). Bulletin of the Chemical Society of Japan 1989, 62 (8) , 2728-2729. https://doi.org/10.1246/bcsj.62.2728
    28. Masakazu Yamashita, Haruyoshi Tashika, Rikisaku Suemitsu. Hydroacylation of Simple Alkyl Vinyl Ketones Using Organotetracarbonylferrates. Chemistry Letters 1989, 18 (4) , 691-692. https://doi.org/10.1246/cl.1989.691
    29. Didier Vanhoye, Fethi Bedioui, André Mortreux, Francis Petit. Conversion of organic halides by CO into aldehydes using electroreduced fe(CO)5. Tetrahedron Letters 1988, 29 (49) , 6441-6442. https://doi.org/10.1016/S0040-4039(00)82367-9
    30. Christine E. L. Headford, Warren R. Roper. Hydride Transfer to Coordinated Carbon Monoxide and Related Ligands. 1986, 513-552. https://doi.org/10.1007/978-1-4613-1785-2_8
    31. S. Nakamura, A. Dedieu. Ab-initio SCF potential energy surfaces for the nucleophilic attack of hydride on coordinated carbon monoxide. Theoretica Chimica Acta 1982, 61 (6) , 587-595. https://doi.org/10.1007/BF02394735
    32. Armin Trenkle, Heinrich Vahrenkamp*. Doppelt phosphor- BZW.arsen-verbrückte hetero-metall-metall-bindungen. Journal of Organometallic Chemistry 1982, 236 (1) , 71-81. https://doi.org/10.1016/S0022-328X(00)86751-0
    33. J.D. Odom. Non-cyclic Three and Four Coordinated Boron Compounds. 1982, 253-310. https://doi.org/10.1016/B978-008046518-0.00005-2
    34. J.A. Gladysz. Transition Metal Formyl Complexes. 1982, 1-38. https://doi.org/10.1016/S0065-3055(08)60519-5
    35. Andrew J. Blakeney, J.A. Gladysz. Preparation and alkylation reactions of K+[(CO)4FeSi(CH3)3]−; Reductive elimination of tetramethylsilane from isolable (CO)4FeRSi(CH3)3 complexes. Inorganica Chimica Acta 1981, 53 , L25-L27. https://doi.org/10.1016/S0020-1693(00)84730-1
    36. Herbert C. Brown, Gary W. Kramer, John L. Hubbard, S. Krishnamurthy. Addition compounds of alkali metal hydrides. Journal of Organometallic Chemistry 1980, 188 (1) , 1-10. https://doi.org/10.1016/S0022-328X(00)83693-1
    37. Rudolf Gompper, Ekkehard Bartmann. Herstellung anionischer übergangsmetall-Komplexe. Liebigs Annalen der Chemie 1980, 1980 (2) , 229-240. https://doi.org/10.1002/jlac.198019800208
    38. Edwin M. Kaiser. Heavier alkali metals. Journal of Organometallic Chemistry 1979, 183 , 107-140. https://doi.org/10.1016/S0022-328X(00)82804-1
    39. D.S. Matteson. Boron I. Carboranes and hydroboration. Journal of Organometallic Chemistry 1979, 180 , 19-63. https://doi.org/10.1016/S0022-328X(00)83785-7
    40. J. A. GLADYSZ, W. TAM. ChemInform Abstract: ONE-FLASK PREPARATION OF ANALYTICALLY PURE DIPOTASSIUM TETRACARBONYLFERRATE. Chemischer Informationsdienst 1978, 9 (43) https://doi.org/10.1002/chin.197843143

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