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    Substrate-Free Gas-Phase Synthesis of Graphene Sheets
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    Applied Science and Technology Graduate Group, University of California, Berkeley, California 94720, National Center for Electron Microscopy, Lawrence Berkeley National Laboratory, Berkeley, California 94720, Los Alamos National Laboratory, Los Alamos, New Mexico 87545, and Department of Mechanical Engineering, University of California, Berkeley, California 94720
    * Corresponding author, [email protected]
    †Applied Science and Technology Graduate Group, University of California.
    ‡National Center for Electron Microscopy.
    §Los Alamos National Laboratory.
    ∥Department of Mechanical Engineering, University of California.
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    Nano Letters

    Cite this: Nano Lett. 2008, 8, 7, 2012–2016
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    https://doi.org/10.1021/nl8011566
    Published June 5, 2008
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    Abstract

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    We present a novel method for synthesizing graphene sheets in the gas phase using a substrate-free, atmospheric-pressure microwave plasma reactor. Graphene sheets were synthesized by passing liquid ethanol droplets into an argon plasma. The graphene sheets were characterized by transmission electron microscopy, electron energy loss spectroscopy, Raman spectroscopy, and electron diffraction. We prove that graphene can be created without three-dimensional materials or substrates and demonstrate a possible avenue to the large-scale synthesis of graphene.

    Copyright © 2008 American Chemical Society

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    Cite this: Nano Lett. 2008, 8, 7, 2012–2016
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    Published June 5, 2008
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