ACS Publications. Most Trusted. Most Cited. Most Read
My Activity
Recently Viewed
You have not visited any articles yet, Please visit some articles to see contents here.
CONTENT TYPES

Figure 1Loading Img

Facile Syntheses of Selenium- and Tellurium-Containing Metal Cubanes, [Cp*M(.mu.3-E)]4 (Cp* = C5Me5; M = Rh, Ir, Ga; E = Se, Te), and X-ray Crystal Structures of (Cp*RhSe)4, (Cp*IrSe)4, (Cp*RhTe)4, (Cp*IrTe)4, and (Cp*GaTe)4

Cite this: Organometallics 1994, 13, 10, 4004–4007
Publication Date (Print):October 1, 1994
https://doi.org/10.1021/om00022a042
ACS Legacy Archive
Article Views
152
Altmetric
-
Citations
LEARN ABOUT THESE METRICS
PDF (484 KB)
Supporting Info (1)»

Note: In lieu of an abstract, this is the article's first page.

Free first page

Supporting Information


Terms & Conditions

Electronic Supporting Information files are available without a subscription to ACS Web Editions. The American Chemical Society holds a copyright ownership interest in any copyrightable Supporting Information. Files available from the ACS website may be downloaded for personal use only. Users are not otherwise permitted to reproduce, republish, redistribute, or sell any Supporting Information from the ACS website, either in whole or in part, in either machine-readable form or any other form without permission from the American Chemical Society. For permission to reproduce, republish and redistribute this material, requesters must process their own requests via the RightsLink permission system. Information about how to use the RightsLink permission system can be found at http://pubs.acs.org/page/copyright/permissions.html.

Cited By

This article is cited by 48 publications.

  1. K. Yuvaraj, Dipak Kumar Roy, Bijan Mondal, Babu Varghese, and Sundargopal Ghosh . Homometallic Cubane Clusters: Participation of Three-Coordinated Hydrogen in 60-Valence Electron Cubane Core. Inorganic Chemistry 2015, 54 (17) , 8673-8678. https://doi.org/10.1021/acs.inorgchem.5b01298
  2. Stephan Schulz, Stefan Heimann, Kevin Kaiser, Oleg Prymak, Wilfried Assenmacher, Jörg Thomas Brüggemann, Bert Mallick, and Anja-Verena Mudring . Solution-Based Synthesis of GeTe Octahedra at Low Temperature. Inorganic Chemistry 2013, 52 (24) , 14326-14333. https://doi.org/10.1021/ic402266j
  3. Shabana Khan, Sakya S. Sen, Herbert W. Roesky, Daniel Kratzert, Reent Michel, and Dietmar Stalke. One Pot Synthesis of Disilatricycloheptene Analogue and Jutzi’s Disilene. Inorganic Chemistry 2010, 49 (20) , 9689-9693. https://doi.org/10.1021/ic101552r
  4. James E. McDonough, Arjun Mendiratta, John J. Curley, George C. Fortman, Serena Fantasia, Christopher C. Cummins, Elena V. Rybak-Akimova, Steven P. Nolan and Carl D. Hoff. Thermodynamic, Kinetic, and Computational Study of Heavier Chalcogen (S, Se, and Te) Terminal Multiple Bonds to Molybdenum, Carbon, and Phosphorus. Inorganic Chemistry 2008, 47 (6) , 2133-2141. https://doi.org/10.1021/ic701611p
  5. Christopher J. Barden,, Patrick Charbonneau, and, Henry F. Schaefer III. Group 13−Group 16 Heterocubanes [RM(μ3-E)]4 (R = H, CH3; M = Al, Ga, In; E = O, S, Se, Te) and Group 13 Cubanes [RM(μ3-M)]4 (R = F, Cl, CH3, NO2; M = Al, Ga, In):  A Structural Study. Organometallics 2002, 21 (17) , 3605-3609. https://doi.org/10.1021/om0202672
  6. Klaus S. Klimek,, Jörg Prust,, Herbert W. Roesky,, Mathias Noltemeyer, and, Hans-Georg Schmidt. Synthesis and Characterization of Tris(trimethylsilyl)methylaluminum Chalcogenides [RAl(μ3-E)]4 (R = (Me3Si)3C; E = Se, Te) and 1-Azaallylgallium Chalcogenides [R‘Ga(μ2-E)]2 (R‘ = (Me3Si)2C(Ph)C(Me3Si)N; E = S, Se, Te). Organometallics 2001, 20 (10) , 2047-2051. https://doi.org/10.1021/om0010520
  7. Hidetake Seino,, Yasushi Mizobe, and, Masanobu Hidai. Preparation of Dinuclear Rhodium and Iridium Complexes with Two Bridging Hydroselenido Ligands and Their Conversion into Tri- and Tetranuclear Selenido Clusters. Organometallics 2000, 19 (18) , 3631-3639. https://doi.org/10.1021/om0004040
  8. Christopher T. Burns,, Pamela J. Shapiro,, Peter H. M. Budzelaar,, Roger Willett, and, Ashwani Vij. Bis(permethylcyclopentadienyl)aluminum Compounds:  Precursors to [Cp*2Al]+ but Not to Cp*3Al. Organometallics 2000, 19 (17) , 3361-3367. https://doi.org/10.1021/om000173x
  9. Joseph L. Stark,, Brian Harms,, Ilse Guzman-Jimenez,, Kenton H. Whitmire,, Régis Gautier,, Jean-François Halet, and, Jean-Yves Saillard. Different Ways To Distort a Tetracapped Tetrahedron on Route to Forming an E4M4 Cubane:  The Case of [E4(Pd(PPh2Me)2)4][Ph2EX2]2 (E = Sb, X = Cl; E = Bi, X = Br). Journal of the American Chemical Society 1999, 121 (18) , 4409-4418. https://doi.org/10.1021/ja982902u
  10. Colin D. Abernethy,, Frank Bottomley,, Robert W. Day,, Andreas Decken,, David A. Summers, and, Robert C. Thompson. Organometallic Oxides:  Preparation and Properties of the Clusters [(η-C5Me5)V(μ3-O)]4 and [(η-C5Me5)V]4(μ-O)6 by Reductive Aggregation of (η-C5Me5)VCl2(O). Organometallics 1999, 18 (5) , 870-879. https://doi.org/10.1021/om9807809
  11. Stephan Schulz,, Edward G. Gillan,, Jean L. Ross,, Lillian M. Rogers,, Robin D. Rogers, and, Andrew R. Barron. Synthesis of Gallium Chalcogenide Cubanes and Their Use as CVD Precursors for Ga2E3 (E = S, Se). Organometallics 1996, 15 (22) , 4880-4883. https://doi.org/10.1021/om960480w
  12. Alec Bigness, Shivaiah Vaddypally, Michael J. Zdilla, Jose L. Mendoza-Cortes. Ubiquity of cubanes in bioinorganic relevant compounds. Coordination Chemistry Reviews 2022, 450 , 214168. https://doi.org/10.1016/j.ccr.2021.214168
  13. Michael J. Zdilla. Electronic Structure of Paramagnetic Iron and Manganese Cluster Compounds: Historical Developments and Current Understanding. 2021,,https://doi.org/10.1016/B978-0-08-102688-5.00052-0
  14. Stefanie Dehnen, Niklas Rinn. Non-oxide p-block (semi-)metal chalcogenide cage compounds. 2021,,https://doi.org/10.1016/B978-0-12-823144-9.00066-2
  15. Debabrata Mukherjee. Aluminium and Galium. 2021,,, 197-213. https://doi.org/10.1016/B978-0-08-102688-5.00020-9
  16. Vimal K. Jain, Rohit Singh Chauhan. New vistas in the chemistry of platinum group metals with tellurium ligands. Coordination Chemistry Reviews 2016, 306 , 270-301. https://doi.org/10.1016/j.ccr.2015.07.009
  17. Chelladurai Ganesamoorthy, Georg Bendt, Dieter Bläser, Christoph Wölper, Stephan Schulz. Te–Te and Te–C bond cleavage reactions using a monovalent gallanediyl. Dalton Transactions 2015, 44 (11) , 5153-5159. https://doi.org/10.1039/C5DT00172B
  18. Maxim N. Sokolov, Pavel A. Abramov. Chalcogenide clusters of Groups 8–10 noble metals. Coordination Chemistry Reviews 2012, 256 (17-18) , 1972-1991. https://doi.org/10.1016/j.ccr.2012.04.009
  19. Simon Aldridge. The Chemistry of the Group 13 Metals in the +3 Oxidation State: Simple Inorganic Compounds. 2011,,, 75-147. https://doi.org/10.1002/9780470976548.ch2
  20. S. V. Volkov, L. B. Khar’kova, Z. A. Fokina, O. G. Yanko, P. E. Strizhak, G. R. Kosmambetova, V. I. Gritsenko, A. M. Korduban. New cluster-type rhodium selenochlorides in oxidative carbonylation of methane. Russian Journal of Applied Chemistry 2007, 80 (2) , 193-200. https://doi.org/10.1134/S107042720702005X
  21. S. Schulz. Gallium, Indium, and Thallium, Excluding Transition Metal Derivatives. 2007,,, 287-342. https://doi.org/10.1016/B0-08-045047-4/00048-0
  22. Andreas Lange, Marek M. Kubicki, Joachim Wachter, Manfred Zabel. Chemistry of Transition-Metal Clusters with Mixed Sb/S Ligands:  Evidence for a Terminal SbS Double Bond in Cp* 3 Rh 3 Sb 2 S 5 (Cp* = C 5 Me 5 ). Inorganic Chemistry 2005, 44 (21) , 7328-7332. https://doi.org/10.1021/ic050493e
  23. V. I. Pekhno, I. N. Stepanenko, S. V. Volkov, Z. A. Fokina, A. M. Korduban. Some properties of rhodium thioselenochloride RhCl4Se6S9 and its thermal conversion products. Russian Journal of Coordination Chemistry 2004, 30 (12) , 859-863. https://doi.org/10.1007/s11173-005-0030-5
  24. Shoken Nagao, Hidetake Seino, Masanobu Hidai, Yasushi Mizobe. Syntheses of a series of trinuclear MIr2 or pentanuclear MIr4 bimetallic bis(selenido) and selenido–sulfido clusters (M=Pd, Pt, Fe, Co) from diiridium μ-bis(hydroselenido) and μ-hydroselenido–hydrosulfido complexes [{(η5-C5Me5)IrCl}2(μ-SeH)(μ-EH)] (E=Se, S). Journal of Organometallic Chemistry 2003, 669 (1-2) , 124-134. https://doi.org/10.1016/S0022-328X(02)02226-X
  25. Andrew I Wallbank, John F Corrigan. Triply bridged dicopper-bis(trimethylsilylchalcogenolates): Synthesis and characterization of the series of helical complexes [(Me 3 SiE-Cu) 2 (µ-Ph 2 PCCPPh 2 -κ 2 P ) 3 ] (E = S, Se, Te). Canadian Journal of Chemistry 2002, 80 (11) , 1592-1599. https://doi.org/10.1139/v02-032
  26. Hidetake Seino, Masanobu Hidai, Yasushi Mizobe. Rational Synthesis and Crystal Structures of Heterometallic-Heterochalcogenido Cubane-Type Clusters [(Cp * M) 2 (MoOCl 2 ){MoCl 2 (dmf)}(μ 3 -S) 2 (μ 3 -Se) 2 ] (M=Rh, Ir). Chemistry Letters 2002, 31 (9) , 920-921. https://doi.org/10.1246/cl.2002.920
  27. Ned J. Hardman, Philip P. Power. Dimeric Gallium Oxide and Sulfide Species Stabilized by a Sterically Encumbered β-Diketiminate Ligand. Inorganic Chemistry 2001, 40 (11) , 2474-2475. https://doi.org/10.1021/ic015506c
  28. Mauricio Valderrama, Raúl Contreras, M. Pilar Lamata, Fernando Viguri, Daniel Carmona, Fernando J. Lahoz, Sergio Elipe, Luis A. Oro. Bis(diphenylphosphino)amine and their dichalcogenide derivatives as ligands in rhodium(III), iridium(III), and ruthenium(II) complexes. Crystal structures of [(η5-C5Me5)MCl{η2-(SePPh2)2N}] (M=Rh, Ir). Journal of Organometallic Chemistry 2000, 607 (1-2) , 3-11. https://doi.org/10.1016/S0022-328X(00)00088-7
  29. Jonathan Parr, Martin B. Smith, Alexandra M.Z. Slawin. The synthesis and crystal structures of the first examples of six-membered inorganic iridacycles containing the [(Ph2PE)2N]− ligand (E=S or Se). Journal of Organometallic Chemistry 1999, 588 (1) , 99-106. https://doi.org/10.1016/S0022-328X(99)00351-4
  30. V. P. Fedin, I. V. Kalinina, D. G. Samsonenko, Y. V. Mironov, M. N. Sokolov, S. V. Tkachev, A. V. Virovets, N. V. Podberezskaya, M. R. J. Elsegood, W. Clegg, A. G. Sykes. Synthesis, Structure, and Properties of Molybdenum and Tungsten Cyano Complexes with Cuboidal M 4 (μ 3 -E) 4 (M = Mo, W; E = S, Se, Te) Cores. Inorganic Chemistry 1999, 38 (9) , 1956-1965. https://doi.org/10.1021/ic980956z
  31. Peter Jutzi, Neil Burford. Structurally Diverse π-Cyclopentadienyl Complexes of the Main Group Elements. Chemical Reviews 1999, 99 (4) , 969-990. https://doi.org/10.1021/cr941099t
  32. Paul J. Dyson, Anthony F. Hill, Alexander G. Hulkes, Andrew J. P. White, David J. Williams. Liganden mit vierwertigem Tellur. Angewandte Chemie 1999, 111 (4) , 573-575. https://doi.org/10.1002/(SICI)1521-3757(19990215)111:4<573::AID-ANGE573>3.0.CO;2-6
  33. Christoph Schnitter, Andreas Klemp, Herbert W. Roesky, Hans-Georg Schmidt, Cord Röpken, Regine Herbst-Irmer, Mathias Noltemeyer. Reactions of Dimethyl[tris(trimethylsilyl)methyl]metalanes of Aluminum and Gallium with H2S and Elemental Chalcogens – Crystal Structures of [RAl(μ-S)]2·2 THF, [RGa(μ3-S)]4, [{RAl(μ3-S)}3MeAl(μ3-S)], [RAlMe(μ-SeMe)]2, and [RGaMe(μ-TeMe)]2 [R = C(SiMe3)3]. European Journal of Inorganic Chemistry 1998, 1998 (12) , 2033-2039. https://doi.org/10.1002/(SICI)1099-0682(199812)1998:12<2033::AID-EJIC2033>3.0.CO;2-I
  34. Max Herberhold, Guo-Xin Jin, Arnold L. Rheingold. The use of half-sandwich iridium dithiolate and diselenolate complexes, Cp*Ir(L)(ER)2 (L=CO, PMe3, PPh3; ER=SPh, SePh, SeMe), for the synthesis of heterodimetallic compounds. The molecular structure of Cp*Ir(CO)(μ-SePh)2[Mo(CO)4]. Journal of Organometallic Chemistry 1998, 570 (2) , 241-246. https://doi.org/10.1016/S0022-328X(98)00739-6
  35. Matthew C. Kuchta, Gerard Parkin. Terminal chalcogenido complexes of Group 13 and 14 elements. Coordination Chemistry Reviews 1998, 176 (1) , 323-372. https://doi.org/10.1016/S0010-8545(98)00123-4
  36. Michael G. Gardiner, Colin L. Raston. Advances in the chemistry of Lewis base adducts of alane and gallane. Coordination Chemistry Reviews 1997, 166 , 1-34. https://doi.org/10.1016/S0010-8545(97)00002-7
  37. Jeffrey R. Eveland, Kenton H. Whitmire. Synthese und Charakterisierung des Cubanclusters [Fe3(CO)9 Te4(μ3-CTeBr4)] mit einer Carbid-Ecke und einer ungewöhnlichen tetraedrischen CTe4-Einheit. Angewandte Chemie 1997, 109 (11) , 1241-1242. https://doi.org/10.1002/ange.19971091116
  38. Matthew C. Kuchta, Gerard Parkin. Terminal Chalcogenido Complexes of Gallium Supported by Tris(3,5-di- tert -butylpyrazolyl)hydroborato Ligation:  [Tp Bu t 2 ]GaE (E = Se, Te). Inorganic Chemistry 1997, 36 (12) , 2492-2493. https://doi.org/10.1021/ic970208u
  39. Urban App, Kurt Merzweiler. Neue metallorganisch substituierte Gallium-Chalkogen-Verbindungen mit Ga4E4-Heterokubanger�st. Synthese und Kristallstrukturen von [{Cp(CO)2Fe}4Ga4E4] (E = S, Se, Te). Zeitschrift f�r anorganische und allgemeine Chemie 1997, 623 (1-6) , 478-482. https://doi.org/10.1002/zaac.19976230175
  40. C. Jeff Harlan, Edward G. Gillan, Simon G. Bott, Andrew R. Barron. tert -Amyl Compounds of Aluminum and Gallium:  Halides, Hydroxides, and Chalcogenides. Organometallics 1996, 15 (26) , 5479-5488. https://doi.org/10.1021/om9605185
  41. Michael G. Richmond. Annual survey of organometallic metal cluster chemistry for the year 1994. Coordination Chemistry Reviews 1996, 156 , 91-138. https://doi.org/10.1016/0010-8545(95)01223-0
  42. Jeffrey R. Eveland, Kenton H. Whitmire. Synthese und Charakterisierung des neuartigen Eisencarbonyl-Tellurchlorid-Clusters [Fe2(CO)6(μ-Cl)(μ-TeCl)2]2[η2,μ2,μ2Te2Cl10] und seine Zersetzung zu [Fe2(CO)6(η2,μ2,μ2-Te4)(μ-TeCl2)]. Angewandte Chemie 1996, 108 (7) , 841-843. https://doi.org/10.1002/ange.19961080726
  43. Carsten Dohmeier, Dagmar Loos, Hansgeorg Schnöckel. Aluminium(I)- und Gallium(I)- Verbindungen: Synthesen, Strukturen und Reaktionen. Angewandte Chemie 1996, 108 (2) , 141-161. https://doi.org/10.1002/ange.19961080204
  44. Jane E. MacIntyre. Ga Gallium. 1996,,, 95-99. https://doi.org/10.1007/978-1-4899-6848-7_20
  45. Claudio Bianchini, Robert W. Zoellner. Activation of Dioxygen by Cobalt Group Metal Complexes. 1996,,, 263-339. https://doi.org/10.1016/S0898-8838(08)60133-6
  46. Max Herberhold, Guo‐Xin Jin, Wolfgang Milius. Pentamethylcyclopentadienyl Iridium Complexes Containing Chalcogenido Ligands: Reactions of Cp * Ir(CO) 2 with Elemental Sulfur and Selenium. Chemische Berichte 1995, 128 (6) , 557-560. https://doi.org/10.1002/cber.19951280605
  47. Werner Uhl, Rene Graupner, Marcus Layh, Uwe Schütz. In4{C(SiMe3)3}4 mit In4-tetraeder und In4Se4{C(SiMe3)3}4 mit In4Se4-heterocubanstruktur. Journal of Organometallic Chemistry 1995, 493 (1-2) , C1-C5. https://doi.org/10.1016/0022-328X(95)05399-A
  48. Michael G. Gardiner, Colin L. Raston, Vicki-Anne Tolhurst. Alane reduction of selenium and tellurium: tertiary amine stabilised dimeric chalcogenides, trans-[{Me 3 N(H)Al(µ-E)} 2 ](E = Se, Te). J. Chem. Soc., Chem. Commun. 1995, 12 (24) , 2501-2502. https://doi.org/10.1039/C39950002501

Pair your accounts.

Export articles to Mendeley

Get article recommendations from ACS based on references in your Mendeley library.

Pair your accounts.

Export articles to Mendeley

Get article recommendations from ACS based on references in your Mendeley library.

You’ve supercharged your research process with ACS and Mendeley!

STEP 1:
Click to create an ACS ID

Please note: If you switch to a different device, you may be asked to login again with only your ACS ID.

Please note: If you switch to a different device, you may be asked to login again with only your ACS ID.

Please note: If you switch to a different device, you may be asked to login again with only your ACS ID.

MENDELEY PAIRING EXPIRED
Your Mendeley pairing has expired. Please reconnect

This website uses cookies to improve your user experience. By continuing to use the site, you are accepting our use of cookies. Read the ACS privacy policy.

CONTINUE