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Preprocessed Monomer Interfacial Polymerization for Scalable Fabrication of High-Valent Cluster-Based Metal–Organic Framework Membranes
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    Preprocessed Monomer Interfacial Polymerization for Scalable Fabrication of High-Valent Cluster-Based Metal–Organic Framework Membranes
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    • Yang Feng
      Yang Feng
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      State Key Laboratory of Heavy Oil Processing, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      College of Chemistry and Chemical Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Zixi Kang*
      Zixi Kang
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      State Key Laboratory of Heavy Oil Processing, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      *Email: [email protected]
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    • Zhikun Wang
      Zhikun Wang
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Zhanning Liu
      Zhanning Liu
      School of Materials Science and Engineering, Shandong University of Science and Technology, Qingdao, Shandong 266590, P. R. China
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    • Q. Jason Niu
      Q. Jason Niu
      The Institute for Advanced Study, Shenzhen University, Shenzhen 518060, P. R. China
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    • Weidong Fan
      Weidong Fan
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      State Key Laboratory of Heavy Oil Processing, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Lu Qiao
      Lu Qiao
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Jia Pang
      Jia Pang
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Hu Chang
      Hu Chang
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Xiaolei Cui
      Xiaolei Cui
      State Key Laboratory of Heavy Oil Processing, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      College of Chemistry and Chemical Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Lili Fan
      Lili Fan
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      State Key Laboratory of Heavy Oil Processing, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Hailing Guo
      Hailing Guo
      State Key Laboratory of Heavy Oil Processing, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
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    • Rongming Wang
      Rongming Wang
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      State Key Laboratory of Heavy Oil Processing, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
    • Dan Zhao*
      Dan Zhao
      Department of Chemical & Biomolecular Engineering, National University of Singapore, Singapore 117585, Singapore
      *Email: [email protected]
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    • Daofeng Sun*
      Daofeng Sun
      School of Materials Science and Engineering, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      State Key Laboratory of Heavy Oil Processing, China University of Petroleum (East China), Qingdao, Shandong 266580, P. R. China
      *Email: [email protected]
      More by Daofeng Sun
    Other Access OptionsSupporting Information (1)

    Journal of the American Chemical Society

    Cite this: J. Am. Chem. Soc. 2024, 146, 49, 33452–33460
    Click to copy citationCitation copied!
    https://doi.org/10.1021/jacs.4c10241
    Published November 14, 2024
    Copyright © 2024 American Chemical Society

    Abstract

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    Current research on emergent membrane materials with ordered and stable nanoporous structures often overlooks the vital facet of manufacturing scalability. We propose the preprocessed monomer interfacial polymerization (PMIP) strategy for the scalable fabrication of high-valent cluster-based metal–organic framework (MOF) membranes with robust structures. Using a roll-to-roll device on commercial polymer supports, Zr-fum-MOF membranes are continuously processed at room temperature through the PMIP approach. These large-area membranes demonstrate the preeminent hydrogen separation capabilities, boasting an order of magnitude of permeance and a thrice-enhanced selectivity when juxtaposed with conventional polymeric membranes. The obtained PMIP-Zr-fum-MOF membranes possess superior stability in water compared with interfacial polymerization (IP)-processed low-valent metal-ion-based ZIF-8 membranes. Moreover, we have implemented the PMIP strategy’s universality to process the other four diverse MOF membranes. The proposal of PMIP significantly advances the scalable fabrication of water-stable high-valent cluster MOF membranes.

    Copyright © 2024 American Chemical Society

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    Supporting Information

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    The Supporting Information is available free of charge at https://pubs.acs.org/doi/10.1021/jacs.4c10241.

    • Detailed synthesis methods, physical measurements and instrumentation, analysis methods, and specific separation performance data (PDF)

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    Cited By

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    This article is cited by 1 publications.

    1. Yiming Zhang, Hang Ben Yin, Lingzhi Huang, Li Ding, Song Lei, Shane G. Telfer, Jürgen Caro, Haihui Wang. MOF membranes for gas separations. Progress in Materials Science 2025, 26 , 101432. https://doi.org/10.1016/j.pmatsci.2025.101432

    Journal of the American Chemical Society

    Cite this: J. Am. Chem. Soc. 2024, 146, 49, 33452–33460
    Click to copy citationCitation copied!
    https://doi.org/10.1021/jacs.4c10241
    Published November 14, 2024
    Copyright © 2024 American Chemical Society

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