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Electrochemical Boron-Doped Diamond Film Microcells Micromachined with Femtosecond Laser: Application to the Determination of Water Framework Directive Metals

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Download Hi-Res ImageDownload to MS-PowerPointCite This:Anal. Chem. 2012, 84, 11, 4805-4811
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    Electrochemical Boron-Doped Diamond Film Microcells Micromachined with Femtosecond Laser: Application to the Determination of Water Framework Directive Metals
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    † University of Lyon, Institute of Analytical Sciences, UMR CNRS 5280, Université Claude Bernard Lyon 1, 43 Boulevard 11 Nnovembre 1918, F-69622, Villeurbanne Cedex, France
    ‡ Irstea, UR MALY, 3bis quai Chauveau, CP 220, F-69336, Lyon Cedex 09, France
    § University of Lyon, Lyon Institute of Nanotechnology, UMR CNRS 5270, Université Claude Bernard Lyon 1, 43 Boulevard 11 Novembre 1918, F-69622, Villeurbanne Cedex, France
    ∥ University of Annaba, Laboratoire EPEV, BP 12, El Hadjar, 23000 Annaba, Algeria
    ⊥ University of Lyon, Laboratoire Hubert Curien, UMR CNRS 5516, Université Jean Monnet Saint-Etienne, Saint-Etienne
    ⊗ Société IMPULSION SAS, 12, Rue Barrouin, 42000 Saint-Etienne
    ○ BVT Technologies a.s., Hudcova 78c, 612 00 Brno, Czech Republic
    *Phone: +33 472448306. Fax: +33 472441206. E-mail: [email protected] (P.N.); [email protected] (N.J.-R.).
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    Analytical Chemistry

    Cite this: Anal. Chem. 2012, 84, 11, 4805–4811
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    https://doi.org/10.1021/ac3003598
    Published April 17, 2012
    Copyright © 2012 American Chemical Society
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    Abstract

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    Planar electrochemical microcells were micromachined in a microcrystalline boron-doped diamond (BDD) thin layer using a femtosecond laser. The electrochemical performances of the new laser-machined BDD microcell were assessed by differential pulse anodic stripping voltammetry (DPASV) determinations, at the nanomolar level, of the four heavy metal ions of the European Water Framework Directive (WFD): Cd(II), Ni(II), Pb(II), Hg(II). The results are compared with those of previously published BDD electrodes. The calculated detection limits are 0.4, 6.8, 5.5, and 2.3 nM, and the linearities go up to 35, 97, 48, and 5 nM for, respectively, Cd(II), Ni(II) Pb(II), and Hg(II). The detection limits meet with the environmental quality standard of the WFD for three of the four metals. It was shown that the four heavy metals could be detected simultaneously in the concentration ratio usually measured in sewage or runoff waters.

    Copyright © 2012 American Chemical Society

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    Analytical Chemistry

    Cite this: Anal. Chem. 2012, 84, 11, 4805–4811
    Click to copy citationCitation copied!
    https://doi.org/10.1021/ac3003598
    Published April 17, 2012
    Copyright © 2012 American Chemical Society
    Request reuse permissions

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