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Multimode Photo-CSTR (Continuous Stirred Tank Reactor) Setup for Heterogeneous Photocatalytic Processes

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Download Hi-Res ImageDownload to MS-PowerPointCite This:Org. Process Res. Dev. 2024, 28, 5, 1683-1689
    Article

    Multimode Photo-CSTR (Continuous Stirred Tank Reactor) Setup for Heterogeneous Photocatalytic Processes
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    • Rizvi Syed Aal E Ali
      Rizvi Syed Aal E Ali
      State Key Laboratory of Molecular & Process Engineering, School of Chemistry and Molecular Engineering, East China Normal University, 3663 North Zhongshan Road, Shanghai 200062, China
      More by Rizvi Syed Aal E Ali
    • Jiaolong Meng
      Jiaolong Meng
      State Key Laboratory of Molecular & Process Engineering, School of Chemistry and Molecular Engineering, East China Normal University, 3663 North Zhongshan Road, Shanghai 200062, China
      More by Jiaolong Meng
    • Xuefeng Jiang*
      Xuefeng Jiang
      State Key Laboratory of Molecular & Process Engineering, School of Chemistry and Molecular Engineering, East China Normal University, 3663 North Zhongshan Road, Shanghai 200062, China
      State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China
      School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, China
      *E-mail: [email protected]
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      Orcidhttps://orcid.org/0000-0002-1849-6572
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    Organic Process Research & Development

    Cite this: Org. Process Res. Dev. 2024, 28, 5, 1683–1689
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    https://doi.org/10.1021/acs.oprd.3c00328
    Published November 15, 2023
    Copyright © 2023 American Chemical Society
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    Abstract

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    Photocatalysis has been comprehensively applied to diverse valuable chemical transformations. However, photocatalytic processes have encountered obstacles in gaining wide acceptance in industry, primarily due to scale-up challenges, especially in heterogeneous systems involving equivalent amounts of solids. We designed a photo-continuous stirred tank reactor (CSTR) protocol for heterogeneous photocatalytic processes, which is capable of multiphasic processes with excellent adaptability. Furthermore, glass-wool-supported photocatalyst was successfully made, applied, and recycled at least 12 times without any decrease in hydroxylation of phenylboronic acid in reactivity, enabling gram scale synthesis with high efficiency in photo-CSTR.

    Copyright © 2023 American Chemical Society

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    Cited By

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    This article is cited by 3 publications.

    1. Hannah L. D. Hayes, Carl J. Mallia. Continuous Flow Chemistry with Solids: A Review. Organic Process Research & Development 2024, 28 (5) , 1327-1354. https://doi.org/10.1021/acs.oprd.3c00407
    2. Émilie Morin, William Neiderer, Corentin Cruché, Oliver Bleton, Charlotte Cave, Shawn K. Collins. A Flow Chemistry Platform for Photochemical Macrocyclization of Peptides. ACS Sustainable Chemistry & Engineering 2024, 12 (16) , 6433-6439. https://doi.org/10.1021/acssuschemeng.4c01441
    3. Yi-Hsuan Tsai, Martin Cattoen, Guillaume Masson, Gabrielle Christen, Lisa Traber, Morgan Donnard, Frédéric R. Leroux, Guillaume Bentzinger, Sylvain Guizzetti, Jean-Christophe M. Monbaliu. On a seamlessly replicable circular photoreactor for lab-scale continuous flow applications. Reaction Chemistry & Engineering 2024, 2 https://doi.org/10.1039/D4RE00109E
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    Organic Process Research & Development

    Cite this: Org. Process Res. Dev. 2024, 28, 5, 1683–1689
    Click to copy citationCitation copied!
    https://doi.org/10.1021/acs.oprd.3c00328
    Published November 15, 2023
    Copyright © 2023 American Chemical Society
    Request reuse permissions

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